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AUTOMATIC QUALITATIVE ANALYSIS METHOD BASED ON SPECTRAL DATA

机译:基于光谱数据的自动定性分析方法

摘要

PURPOSE:To identify existing elements automatically without comparing an energy level corresponding to the peak of spectrums with a standard spectrum table by projecting a charged particle beam on a sample, separating charged electrons generated by said projection in correspondence with energy or mass, detecting a signal, and performing qualitative analysis of the sample based on the signal. CONSTITUTION:An electron EB is projected on a sample 3. Generated Auger electrons AE are separated in correspondence with energy with a spectroscope 4. A signal which is detected with a detector 5 is supplied to an AD converter 7 through an amplifier 6. The converted signal undergoes automatic qualitative analysis in a central processing unit 8. The result is stored in a memory device 9. The result is displayed on a spectrum display device 10. The background is removed from the processed signal in the CPU 8, and the peak is taken out. The position of the peak is obtained. Element-name data are read out of a table 11 wherein the element-name data corresponding to the position are stored. Whether the data correspond to the rank of the noted peak or not is judged.
机译:目的:通过将带电粒子束投射到样品上,分离与能量或质量对应的,由所述投射产生的带电电子,检测信号,从而自动识别现有元素,而无需将与光谱峰值相对应的能级与标准光谱表进行比较,并根据信号对样品进行定性分析。组成:一个电子EB投射在一个样品3上。所产生的俄歇电子AE与分光镜4相对应地被分离。一个由检测器5检测到的信号通过一个放大器6被提供给一个AD转换器7。信号在中央处理单元8中进行自动定性分析。结果存储在存储设备9中。结果显示在频谱显示设备10中。在CPU 8中从处理后的信号中去除背景,并且峰值为带走。获得峰的位置。从表11中读出元素名称数据,其中存储了与该位置相对应的元素名称数据。判断数据是否对应于所述峰的等级。

著录项

  • 公开/公告号JPH02262040A

    专利类型

  • 公开/公告日1990-10-24

    原文格式PDF

  • 申请/专利权人 JEOL LTD;

    申请/专利号JP19890083778

  • 发明设计人 SEKINE SATORU;

    申请日1989-03-31

  • 分类号G01N23/227;H01J49/00;

  • 国家 JP

  • 入库时间 2022-08-22 06:25:20

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