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PROCESS TO PROVIDE DISTINCT SOLID PARTICLES WITH A METAL COMPOUND COATING AND DISTINCT SOLID PARTICLES
PROCESS TO PROVIDE DISTINCT SOLID PARTICLES WITH A METAL COMPOUND COATING AND DISTINCT SOLID PARTICLES
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机译:提供具有金属复合涂层的离散固体颗粒和离散固体颗粒的过程
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摘要
Process for coating discrete particles (preferably ceramic particles) with metal compounds, namely metal oxides and metal nitrides. The process comprises forming a solution of an organometallic compound in a substantially anhydrous solvent that is substantially immiscible with water at ambient temperature, coating the particles with the solution and maintaining the particles substantially separate from each other while removing the solvent from the coating solution, e.g. by atomizing a slurry of the particles and the solution into a volume of heated gas. The resulting particles coated with the organometallic compound are then heated to a temperature at which the organometallic compound is converted to the corresponding metal oxide. If the final coating is to consist of a metal nitride, a carbon precursor (e.g. petroleum pitch) is also dissolved in the anhydrous solvent before the particles are coated, and then the oxide formed in the heating step is converted to the nitride by further heating at high temperature in the presence of nitrogen or a nitrogen precursor. The process is capable of producing ceramic particles coated with a uniform, continuous, non-porous layer of metal oxide or nitride suitable for use, for example, as reinforcements for ceramic or metallic composite materials.
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机译: (54)标题:具有硅酸盐涂层的固体颗粒(54):FESTKoRPERPARTKEL MIT SILKATBESCHICHTUNG(57)摘要:本发明涉及一种具有二氧化硅涂层的固体颗粒的生产方法,其包括以下步骤:将固体颗粒分散为将其涂覆在水性介质中以产生固体颗粒分散体,通过缓冲系统调节固体颗粒分散体的pH以产生缓冲的固体颗粒分散体,并向缓冲的固体颗粒分散体中添加碱性硅酸盐溶液以形成二氧化硅在涂覆期间将其涂覆在固体颗粒上,其中选择缓冲体系和碱性硅酸盐溶液的量,使得在添加碱性硅酸盐溶液之前和在添加完成之后,缓冲的固体颗粒分散体的pH至少为7.0。碱性硅酸盐溶液的最大含量为11.0。固体颗粒优选是无机固体,特别是