PREPARATION AND PURIFICATION METHOD OF 2-NYTRO-5-PHENILTIOMETHOXYACETANYLIDE

摘要

2-nitro-5-phenyl-thio-methoxy-acet-anilide is prepd. in a single step, by acylating 2-nitro-5-phenyl-thio-aniline with methoxy-acetyl-chloride (15% soln. in benzene). Washing is carried out with isopropanol on the filtered reaction mix