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Two-stage process for preparing aromatic polyamide film

机译:制备芳族聚酰胺薄膜的两步法

摘要

A process for preparing aromatic polyamide film wherein an aromatic diamine and an aromatic diacidchloride are dissolved in an amide polymerization solvent containing an inorganic salt, a partial polymerization is effected at a low temperature to form an optically anisotropic liquid crystalline prepolymer dope, continuously extruding through a film die under a draw ratio or subjecting to a shear and contacting the prepolymer with a second solvent which is a polymerization accelerating-precipitation solvent to obtain an aromatic polyamide film free of crystal defect layer perpendicular to the film axis and having high strength and a high degree of molecular orientation.
机译:一种制备芳族聚酰胺薄膜的方法,其中将芳族二胺和芳族二酰氯溶解在含有无机盐的酰胺聚合溶剂中,在低温下进行部分聚合以形成光学各向异性的液晶预聚物涂料,并通过连续挤出。薄膜模在拉伸比下或经受剪切作用并使预聚物与作为聚合促进沉淀溶剂的第二种溶剂接触,以获得无垂直于薄膜轴的晶体缺陷层并具有高强度和高强度的芳族聚酰胺薄膜。分子取向度。

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