首页> 外国专利> Process for the preparation of eventually deuterated cis-inositol, meso-inositol, epi-inositol and/or cis-quercitol

Process for the preparation of eventually deuterated cis-inositol, meso-inositol, epi-inositol and/or cis-quercitol

机译:最终氘化的顺式肌醇,中观肌醇,表肌醇和/或顺式槲皮醇的制备方法

摘要

The invention relates to a process for the preparation of optionally deuterated cis-inositol, meso-inositol, epi-inositol and/or cis-quercitol. This process consists in subjecting tetrahydroxybenzoquinone to catalytic hydrogenation, using a palladium-based catalyst, and in then recovering cis-inositol by separating the products obtained by chromatography on a cation-exchange resin, for example a resin in the Ca2+ form. Preferably, there is used as catalyst, at the beginning of the reaction, palladium which has been reduced beforehand in a neutral medium.
机译:本发明涉及一种制备任选地氘化的顺式肌醇,中观肌醇,表肌醇和/或顺式槲皮醇的方法。该方法包括使用钯基催化剂对四羟基苯醌进行催化氢化,然后通过分离在阳离子交换树脂上层析得到的产物,例如Ca 2+形式的树脂,来回收顺式肌醇。 。优选地,在反应开始时,使用已在中性介质中预先还原的钯作为催化剂。

著录项

  • 公开/公告号EP0524082B1

    专利类型

  • 公开/公告日1995-10-18

    原文格式PDF

  • 申请/专利权人 COMMISSARIAT A LENERGIE ATOMIQUE;

    申请/专利号EP19920402031

  • 发明设计人 ODIER LEON;

    申请日1992-07-15

  • 分类号C07C35/16;C07C29/17;C07C29/76;

  • 国家 EP

  • 入库时间 2022-08-22 04:13:33

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