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A method for the production of toluylene diisocyanate, special mixtures of toluene diamine and water and their use for the preparation of toluylene diisocyanate

机译:一种甲苯二异氰酸酯的生产方法,甲苯二胺和水的特殊混合物及其在制备甲苯二异氰酸酯中的用途

摘要

toluylendiisocyanat nitration of toluene to be dinitrotoluol, hydrogenation of the dinitrotoluols, possibly in the presence of a solvent or diluent, to a rohlu00f6sung from toluylendiamin and reaktionswasser,reappraisal of the toluylendiamin - rohlu00f6sung to dry toluylendiamin of commercial quality and phosgenierung of toluylendiamins to toluylendiisocyanat produced, with the destillative reappraisal of the toluylendiamin - rohlu00f6sung to anhydrous toluylendiamin,if necessary, after complete or partial resolution of separation of the solvent or diluent in a first manufacturing facility with a water content of 1 to 40 wt.%, preferably 2 to 10% by weight.-% is interrupted, the resulting mixture in liquid form to another plant is transported, where the destillative drying of the toluylendiamins is completed, where appropriate, further aufarbeitungsstufen be connected and then the toluylendiamin in to fa nder way to toluylendiisocyanat phosgeniert.the invention concerns also a $toluylendiamin and mixtures of water with a point of maximum 95u00b0c and their use for the production of toluylendiisocyanat, preferably in a place, the place of manufacture of mixtures of water and toluylendiamin differences hiedlich.
机译:甲苯的二异氰酸酯被硝化为二硝基甲苯,二硝基甲苯的氢化,可能在溶剂或稀释剂存在下,由甲苯二胺和再水合剂制得的rohl,重新评估甲苯二胺的质量-甲苯二胺的质量和干燥的甲苯二酚的质量甲苯二胺至甲苯二异氰酸酯的生产,并在必要时在水含量为1至40 wt。的第一生产设施中完全或部分分离溶剂或稀释剂后,将甲苯胺二胺-rohlf6进行蒸馏性重新评估为无水甲苯二胺。中断%,优选2-10重量%。将液体形式的所得混合物运输到另一工厂,在其中甲苯胺二胺的蒸馏干燥完成,在适当的情况下,进一步连接aufarbeitungsstufen,然后将甲苯胺二胺加入本发明涉及一种甲苯胺的进一步制备方法。黄连二胺和最高点为95的水的混合物及其在生产甲苯基异氰酸酯中的用途,优选在生产水和甲苯二胺二甲酸酯差异混合物的地方。

著录项

  • 公开/公告号DE19528781A1

    专利类型

  • 公开/公告日1997-02-06

    原文格式PDF

  • 申请/专利权人 BAYER AG DE;

    申请/专利号DE1995128781

  • 申请日1995-08-04

  • 分类号C07C211/50;C07C265/12;C07C209/90;C07C263/10;

  • 国家 DE

  • 入库时间 2022-08-22 03:15:14

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