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The porous graphite quality carbon granular material and uses that the support material null for the chromatography

机译:多孔石墨质碳粒材料,并使用该载体材料进行色谱分离

摘要

PURPOSE:To obtain a suitable supporting body for high speed liquid chromatography having nonpolar and stable chemical properties and high compressive strength by providing a granular graphitic carbon material having respectively specified grain size, specific surface area, porosity, and interlamellar spacing. CONSTITUTION:A powdered carbonaceous material having an average grain size of 1-1000mum, preferably 5-100mum, a specific surface area of =10m2/g, preferably 50-400m2/g, a porosity of 5-60%, preferably 20-50%, and an average interlamellar spacing (d002) of carbon determined by an X-ray analytic method of 3.35-3.42Angstrom , preferably 3.35-3.40Angstrom , is formed into a granular porous graphitic carbon material useful as a supporting material for chromatography. This granular material has superior mechanical strength, particularly =500kg/cm2 compressive strength, and, by using this material as a supporting material for high speed liquid chromatography in particular, highly efficient analysis is carried out.
机译:目的:通过提供具有分别规定的晶粒尺寸,比表面积,孔隙率和层间间距的粒状石墨碳材料,以获得具有非极性和稳定化学性质以及高抗压强度的高速液相色谱的合适支撑体。组成:一种粉末状碳质材料,平均粒径为1-1000μm,优选为5-100μm,比表面积为≥10m2 / g,优选为50-400m 2 / g,孔隙率为5-通过X射线分析法确定的碳的平均层间距(d002)为3.35-3.42埃,优选为3.35-3.40埃,其中碳的平均层间距为60%,优选为20-50%,形成颗粒状多孔石墨碳材料,可用作色谱的支撑材料。该粒状材料具有优异的机械强度,特别是≥500kg/ cm 2的抗压强度,并且通过将该材料特别用作高速液相色谱的支撑材料,可以进行高效的分析。

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