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METHOD FOR PRODUCING AGGLOMERATE-FREE NANOSCALE IRON OXIDE PARTICLES WITH HYDROLYSIS-RESISTANT COATING

机译:耐水解涂层的无团聚纳米氧化铁颗粒的制备方法

摘要

A process for preparing an agglomerate-free suspension of nanosize iron-containing oxide particles coated in a stable manner comprises preparing an aqueous suspension of nanosize iron-containing oxide particles which are partially or completely in the form of agglomerates; adding a trialkoxysilane and a water-miscible polar organic solvent which has a boiling point at least 10° C. higher than the boiling point of water; treating the resulting suspension with ultrasound until at least 70% of the particles present are in the range of ±20% of the average particle diameter; removing the water by distillation under the action of ultrasound; and separating the non-disintegrated agglomerates.
机译:一种以稳定方式涂覆的纳米级含铁氧化物颗粒的无附聚物悬浮液的制备方法,包括制备部分或全部以附聚物形式存在的纳米级含铁氧化物颗粒的水悬浮液;加入三烷氧基硅烷和沸点比水的沸点高至少10℃的与水混溶的极性有机溶剂;用超声波处理所得的悬浮液,直到存在的至少70%的颗粒在平均粒径的±20%范围内;在超声作用下通过蒸馏除去水;并分离未分解的团块。

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