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Separation and Purification System of phytochemicals by mild-temperature extraction vessel and Vacuum Chromatography

机译:中温提取容器和真空色谱法分离植物化学制品的系统

摘要

The invention tree (樹木) or number of the combined extracts (混合 抽出 物) of higher plants (高等植物) in a relatively simple process, cheap and, in a high yield, by extraction and separation of flavonoids flow or terpenoid acids or trace purification of the kind in alkaloids pure state, the present invention relates to a method for the production. The production method according to the present invention is crushing the sample to be extracted with methanol and then a solution of water at a constant rate, the steps, the nature of the material to be separated to extract the device shown in the figure 1 at an appropriate temperature aqueous solution and by the step of: in an organic solvent fractions (fractionation), [figure 2] the primary purification step using a vacuum chromatography apparatus to obtain a fraction of the desired substance in large quantities, and finally Kalam or high performance liquid chromatography (HPLC) as shown in the present invention been made in two steps of purification tea is characterized by high purity that can be purified (純度) in large quantities to facilitate (容易) the plant material.
机译:通过相对简单的过程,廉价且高收率的黄酮类流或萜类酸或痕量类黄酮的提取和分离,发明树(树木)或高等植物(高等植物)的混合提取物(混合抽出物)的数量纯化生物碱纯态的种类,本发明涉及一种生产方法。根据本发明的生产方法是先将要提取的样品先用甲醇压碎,然后将水溶液以恒定的速度粉碎,然后按图1所示的步骤将要分离的材料的性质,步骤,图1所示的装置进行粉碎。适当温度的水溶液,并通过以下步骤:在有机溶剂馏分中(馏分),[图2]使用真空色谱仪的初步纯化步骤可大量获取所需物质的馏分,最后获得卡拉姆或高性能如本发明所示的液相色谱法(HPLC)是通过两步纯化制成的,茶的特征在于高纯度,可以大量纯化(纯度)以促进(容易)植物原料。

著录项

  • 公开/公告号KR19990083812A

    专利类型

  • 公开/公告日1999-12-06

    原文格式PDF

  • 申请/专利权人 현승일;

    申请/专利号KR19990033000

  • 发明设计人 김영균;

    申请日1999-08-11

  • 分类号C07B63/00;

  • 国家 KR

  • 入库时间 2022-08-22 01:46:33

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