首页> 外国专利> ENERGETIC PLASTICIZER COMPRISING A EUTECTIC MIXTURE OF BIS (2,2-DINITROPROPYL) FORMAL, 2,2 DINITROPROPYL-2,2-DINITROBUTYLFORMAL AND BIS (2,2-DINITROBUTYL) FORMAL, AND PROCESS FOR PREPARING THE SAME

ENERGETIC PLASTICIZER COMPRISING A EUTECTIC MIXTURE OF BIS (2,2-DINITROPROPYL) FORMAL, 2,2 DINITROPROPYL-2,2-DINITROBUTYLFORMAL AND BIS (2,2-DINITROBUTYL) FORMAL, AND PROCESS FOR PREPARING THE SAME

机译:含BIS(2,2-二苯甲基)甲醛,2,2 DINITROPYL-2,2-二苯甲基甲醛和BIS(2,2-DINITROBUTYL)甲醛的共混物的能量增塑剂,及其制备方法

摘要

The invention relates to an energetic plasticizer comprising bis (2,2-dinitropropyl) formal, 2,2-dinitropropyl-2,2-dinitrobutylformal and bis (2,2-dinitrobutyl) formal in a molar ratio of 20 to 68. % / 28 to 50% / 4 to 30% and a process for its preparation which comprises dissolving 2, 2-dinitropropanol and 2,2-dinitrobutanol in an organic solvent to form an organic solution in which the molar ratio from 2, 2-dinitropropanol to 2, 2-dinitrobutanol is 3: 1-6: 1, adding to the organic solution a sulfuric acid solution in which a source of formaldehyde has been dissolved, while the temperature the reaction mixture is kept below 20 ° C, and the separation and purification of the product from the reaction mixture.
机译:本发明涉及一种能量增塑剂,其包含摩尔比为20至68.%的双(2,2-二硝基丙基)甲醛,2,2-二硝基丙基-2,2-二硝基丁基甲醛和双(2,2-二硝基丁基)甲醛。 28至50%/ 4至30%及其制备方法,该方法包括将2,2-二硝基丙醇和2,2-二硝基丁醇溶解在有机溶剂中以形成有机溶液,其中2,2-二硝基丙醇与2,2-二硝基丁醇为3:1-6:1,将硫酸溶液溶解于甲醛溶液中并添加到有机溶液中,同时将反应混合物的温度保持在20°C以下,从反应混合物中纯化产物。

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