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METHOD FOR FABRICATING BISMUTH GERMANIUM OXIDES CRYSTAL
METHOD FOR FABRICATING BISMUTH GERMANIUM OXIDES CRYSTAL
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机译:铋酸铋晶体的制备方法
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摘要
PURPOSE: A fabrication method of bismuth germanium oxides crystal to exclude inclusion-induced crystalline defects is provided. CONSTITUTION: In a manufacturing method of bismuth germanium oxides crystal where seed crystals for bismuth germanium oxides come into contact with melt in crucible, the method includes step of charging 1500 g of starting material in the range of 39.2-39.7 mole% Bi2O3 in platinum crucible and subsequently melting the starting material by induction heat; contacting seed crystals for bismuth germanium oxides in 110 crystal direction with melt obtained in above step and subsequently pulling up the seed crystals at an elevation rate of 3.05 mm/h and at a rotation speed of 45 rpm in atmosphere; and separating the pulled-up bismuth germanium oxides crystal and subsequently cooling it at a cooling rate of 20 deg.C/h to obtain transparent bismuth germanium oxides crystal.
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机译:目的:提供一种铋锗氧化物晶体的制造方法,以排除夹杂物引起的晶体缺陷。组成:在一种铋锗氧化物晶体的制造方法中,铋锗氧化物的种晶与坩埚中的熔体接触,该方法包括以下步骤:将1500 g起始原料装入39.2-39.7摩尔%Bi2O3的铂坩埚中随后通过感应加热将原料熔化;使氧化锗锗的晶种在上述步骤中在<110>晶体方向上与熔融物接触,随后在大气中以3.05 mm / h的升高速率和45 rpm的转速提起晶种;分离出提拉的铋锗氧化物晶体,随后以20℃/ h的冷却速度冷却,得到透明的铋锗氧化物晶体。
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