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DETECTOR FOR HIGH-PERFORMANCE LIQUID CHROMATOGRAPH

机译:高效液相色谱检测器

摘要

PROBLEM TO BE SOLVED: To provide a detector for a high-performance liquid chromatograph which has a large S/N ratio, which has a sufficient dynamic range and which can perform a high-sensitivity detection.;SOLUTION: A mobile phase and a sample reach a measuring flow channel 16, monochromatic light is irradiated from a spectroscope 8 so as to be detected by a detecting element 13, and a detection signal is sent to a control part 19. The mobile phase and the sample are moved further to a measuring flow channel 17, and monochromatic light is irradiated from a spectroscope 3 so as to be detected by a detecting element 12. In the control part 19, the required time in which the mobile phase and the sample are moved to the flow channel 17 from the flow channel 16 is calculated on the basis of the liquid feed speed of a pump and on the basis of the internal volume of the flow channel 16. The detection signal obtained by the detecting element 13 is added to a detection signal obtained by the detecting element 12 after the required time in which the mobile phase and the sample are moved from the flow channel 16 to the flow channel 17, their added value is divided by two, and a mean value is calculated by the control part 19.;COPYRIGHT: (C)2003,JPO
机译:要解决的问题:提供一种用于高性能液相色谱的检测器,该检测器具有较大的信噪比,足够大的动态范围并可以执行高灵敏度检测。解决方案:流动相和样品到达测量流道16,从分光镜8发出单色光,以便由检测元件13进行检测,并将检测信号发送到控制部件19。流动相和样品进一​​步移至测量流动通道17,从分光镜3照射单色光,以便由检测元件12检测。在控制部19中,将流动相和样品从流动通道17移动到流动通道17所需的时间。流动通道16是基于泵的液体进给速度和流动通道16的内部体积来计算的。由检测元件13获得的检测信号被添加到由de元件获得的检测信号中。在流动相和样品从流动通道16移动到流动通道17所需的时间之后,检测元件12将它们的相加值除以二,并由控制部件19计算平均值。 :(C)2003,日本特许厅

著录项

  • 公开/公告号JP2003014720A

    专利类型

  • 公开/公告日2003-01-15

    原文格式PDF

  • 申请/专利权人 SHIMADZU CORP;

    申请/专利号JP20010202860

  • 发明设计人 HAYAKAWA SADAHIRO;IWATA YOUSUKE;

    申请日2001-07-04

  • 分类号G01N30/74;G01N30/78;G01N30/86;

  • 国家 JP

  • 入库时间 2022-08-22 00:16:44

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