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Method of producing nanophase Cu-Al2O3 composite powder

机译:纳米相Cu-Al2O3复合粉末的生产方法

摘要

The present invention relates to a method of producing nanophase Cu—Al2O3 composite powder by means of 1) the producing precursor powders by centrifugal spray drying process using the water base solution, in which Cu-nitrate (Cu(NO3)23H2O) and Al-Nitrate (Al(NO3)39H2O) are solved to the point of final target composition (Cu-1 wt %/Al2O3),2) the heat treatment process (desaltation process) at the 850° C. for 30 min in air atmosphere to remove the volatile components such as the moisture and NO3 group in precursor powder and simultaneously to synthesize the nano CuO—Al2O3 composite powders by the oxidation of corresponded metal components and 3) the reduction heat treatment of CuO at 200° C. for 30 min in reducing atmosphere to produce the final nanophase Cu—Al2O3 composite powders with the size below 20 nm.
机译:本发明涉及一种通过以下方式制备纳米相Cu& Al 2 O 3 复合粉末的方法,该方法是:1)使用水基离心喷雾干燥法制备前体粉末。解决方案,其中硝酸铜(Cu(NO 3 2 3H 2 O)和硝酸铝(Al(NO 3 3 9H 2 O)分解到最终目标组成点(Cu-1 wt%/ Al 2 O 3 ),2)在850°C的热处理过程(脱盐过程);空气中保持30分钟,以除去前体粉末中的挥发性成分,例如水分和NO 3 基团,同时合成纳米CuO&Ald 2 O <通过相应金属成分的氧化而形成Sub> 3 复合粉末,以及3)在200°C下还原CuO的热处理;在还原性气氛中保持30分钟,以产生尺寸小于20nm的最终纳米相Cu& Al 2 O 3 复合粉末。

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