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A device for the determination of element - concentrations in samples by means of high-resolution spectrometer

机译:一种通过高分辨率光谱仪测定样品中元素浓度的装置

摘要

The invention relates to a device (10) for identifying concentrations of elements in samples. Said device comprises a continuous radiation source (14), a high-resolution spectrometer (28), an imaging optical system (16, 22, 26) which images the radiation of the radiation source (14) onto the entrance gap (52) of the spectrometer (28), and a detector (32) in the exit gap plane of the spectrometer (28). Said detector is provided with a plurality of detector elements which are used to scan a spectral range in which at least one spectral line of at least one element to be identified lies, said scanned range also including a surrounding area of said spectral line. The device (10) is further characterized in that the imaging optical system (16, 22, 26) generates at least three real images of the radiation source (14), that a sample compartment (34) is provided at the site of a first real image (18) and a sample compartment (36) at the site of an additional real image (24). The atomization device may be a graphite tube (36) or a flame (34) and emission can be induced by ICP torch. The spectrometer (28) is an echelle spectrometer.
机译:本发明涉及一种用于识别样品中元素浓度的装置(10)。所述设备包括连续辐射源(14),高分辨率光谱仪(28),成像光学系统(16、22、26),该成像光学系统将辐射源(14)的辐射成像到光阑的入射间隙(52)上。光谱仪(28),以及位于光谱仪(28)出口间隙平面的检测器(32)。所述检测器设置有多个检测器元件,所述多个检测器元件用于扫描光谱范围,在所述光谱范围中至少要识别的元素的至少一条光谱线位于该光谱范围中,所述扫描范围还包括所述光谱线的周围区域。装置(10)的特征还在于,成像光学系统(16、22、26)产生辐射源(14)的至少三个真实图像,在第一位置上设置样品室(34)。真实图像(18)和位于另一个真实图像(24)位置的样品室(36)。雾化装置可以是石墨管(36)或火焰(34),并且可以通过ICP炬来引发发射。光谱仪(28)是阶梯光谱仪。

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