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Process for synthesizing and controlling the particle size and particle size distribution of a molecular sieve
Process for synthesizing and controlling the particle size and particle size distribution of a molecular sieve
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机译:合成和控制分子筛的粒度和粒度分布的方法
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摘要
Applicants have developed a continuous process for synthesizing various molecular sieves. The process enables one to control both the particle size and particle size distribution. Any of the molecular sieves represented by the empirical formula on an anhydrous basis: rR2O:(SixAlyPz)O2, where R is at least one structure directing agent, “r”, “x”, “y” and “z” are the mole fractions of R, Si, Al and P respectively, can be prepared using this process. The process involves continuously adding separate streams comprising reactive sources of at least each framework element into a continuous crystallization reactor. Either interstage backmixing is introduced or the number of stages is adjusted in order to control particle size.
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机译:申请人已经开发了用于合成各种分子筛的连续方法。该方法使人们能够控制粒度和粒度分布。用无水经验公式表示的分子筛:rR 2 Sub> O:(Si x Sub> Al y Sub> P z Sub>)O 2 Sub>,其中R是至少一种结构导向剂,“ r”,“ x”,“ y”。和“ z”分别使用R,Si,Al和P的摩尔分数可以使用该方法制备。该方法涉及将包含至少每个骨架元素的反应性源的单独的料流连续添加到连续结晶反应器中。引入级间回混或调节级数以控制粒度。
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