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PARTICULATE HYDROPHOBIC POLYMER, PRODUCTION PROCESS THEREFOR AND COLUMN FOR REVERSED-PHASE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY

机译:颗粒状疏水性聚合物,制备方法及其逆相高效液相色谱柱

摘要

Reacting the particulate crosslinked polymer (A) and the crosslinkable epoxy compound (B) having a hydroxyl group and, after the hydrolysis of the epoxy bond, reacting the epoxy compound (C) having a compound with a total carbon number of 6-40 having a hydroxyl group obtained analysis method using a particulate hydrophobic polymer, a method of manufacturing the same, a column for reversed-phase liquid chromatography, and the column is prepared by. Notably the use of particulate hydrophobic polymers of this invention have a high acid / alkali resistance, the swelling and shrinkage of the particulate polymer itself is reduced, even if the eluent is variously exchanged in the column without the column efficiency among various solvents not degrade polycyclic aromatic it is possible to obtain a sharp chromatogram for a compound.
机译:使颗粒状交联聚合物(A)与具有羟基的可交联环氧化合物(B)反应,并且在环氧键水解之后,使具有总碳原子数为6-40的化合物的环氧化合物(C)反应,使用颗粒状疏水性聚合物得到的羟基的分析方法,其制造方法,反相液相色谱用柱,以及通过该柱来制备。值得注意的是,使用本发明的粒状疏水性聚合物具有高的耐酸/碱性,即使在没有各种溶剂之间的柱效的情况下在柱中以各种方式交换洗脱液,也不会降低粒状聚合物本身的溶胀和收缩,不会降解多环芳香族化合物,可以获得清晰的色谱图。

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