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PREPARATION METHOD OF INDIUM TIN OXIDE NANO-POWDER USING FLAME SPRAY PYROLYSIS

机译:火焰喷涂热解法制备氧化铟锡纳米粉的方法

摘要

PURPOSE: A method for preparing an indium tin oxide nano-powder by using flame spray pyrolysis is provided, to obtain an indium tin oxide nano-powder having a size of 10-25 nm by aerosol method. CONSTITUTION: The method comprises the step of injecting a liquid drop comprising a reactant which is a mixture of indium nitrate and tin chloride dissolved in distilled water, oxygen, hydrogen and air simultaneously into a quintuple-tube flame reactor and generating flame of 900 deg.C or more to prepare an indium tin oxide nano-powder having an average particle size of 10-25 nm. Preferably the first tube(21) flows in 7 vol% of 0.4-0.8 M reactant, the second tube(22) flows in 3 vol% of argon, the fourth tube(24) flows in 20 vol% of oxygen, the third tube(23) flows in 13-20 vol% of hydrogen, and the fifth tube(25) flows in air, and the total flux is controlled by controlling the flux of air at the fifth tube.
机译:目的:提供一种利用火焰喷涂热解法制备氧化铟锡纳米粉的方法,通过气溶胶法制得尺寸为10-25nm的氧化铟锡纳米粉。组成:该方法包括以下步骤:将包含反应物的液滴注入五重管火焰反应器中,该反应物是溶解在蒸馏水,氧气,氢气和空气中的硝酸铟和氯化锡的混合物,同时产生900度的火焰。 C或更高的温度以制备平均粒径为10-25nm的铟锡氧化物纳米粉。优选地,第一管(21)以0.4-0.8M反应物的7体积%流动,第二管(22)以3体积%的氩气流动,第四管(24)以20体积%的氧流动,第三管(23)以13〜20vol%的氢流动,第五管(25)在空气中流动,通过控制第五管处的空气通量来控制总通量。

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