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METHOD OF PRODUCTION OF CATALYST FOR OIL FRACTIONS HYDROUPGRADING

机译:用于油馏分加水合的催化剂的生产方法

摘要

FIELD: chemical and petrochemical industries. SUBSTANCE: invention presents a method of preparation of the catalyst for hydroupgrading of oil fractions by injection into the alumina carrying agent of the phase-forming promoters from a list of aluminosilicates of amorphous and crystalline type, phosphates of compounds of boron, titanium, zirconium, rare earth elements and active components like NiO and MoO3 and / or WO3 by impregnation of the carrying agent with an aqueous solution of salts Ni and Mo and / or W, provided that the impregnation solution is prepared by mixing of an aqueous solution of nickelous nitrate and an aqueous solution of an ammonium molybdate and / or an ammonium tungstate, pre-stabilized by the strong inorganic acids like hydrogen superoxide, hydrogen peroxide, nitric acid, orthophosphoric acid, or their blends; NiO and MoO3 and / or WO3, or MoO3 and WO3 are brought into the carrying agent by impregnation preferably from solutions with concentration by NiO - 80-200 g/l, by MoO3 - 160-250 g/l, and / or by WO3 160-420 g/l, or by MoO3 and WO3 200-420 g/l. EFFECT: catalysts have high strength and activity in process of hydroupgrading of oil fractions. 2 cl, 4 ex, 2 tbl
机译:领域:化学和石化工业。物质:本发明提供了一种方法,该方法用于通过将无定形和结晶型硅铝酸盐,硼,钛,锆化合物的磷酸盐,稀土元素和活性成分,如NiO和MoO 3 和/或WO 3 ,是通过用Ni和Mo和/或W盐的水溶液浸渍载剂来实现的,只要浸渍溶液是通过将硝酸亚硝酸盐水溶液和钼酸铵和/或钨酸铵水溶液混合制备的,并用强无机酸(如过氧化氢,过氧化氢,硝酸,正磷酸)预先稳定酸或其混合物; NiO和MoO 3 和/或WO 3 ,或MoO 3 和WO 3 被带入载体最好从浓度为NiO-80-200 g / l,MoO 3 -160-250 g / l和/或WO 3 160- 420 g / l,或MoO 3 和WO 3 200-420 g / l。效果:催化剂在油馏分的加氢改性过程中具有很高的强度和活性。 2 cl,4 ex,2汤匙

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