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METHOD FOR PREPARING COHESIVE AGENT OF POLYALUMINUM HYDROXY CHLORO-SULFATE SILICATE FOR WATER-TREATMENT AND COHESIVE AGENT PREPARED THEREBY
METHOD FOR PREPARING COHESIVE AGENT OF POLYALUMINUM HYDROXY CHLORO-SULFATE SILICATE FOR WATER-TREATMENT AND COHESIVE AGENT PREPARED THEREBY
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机译:一种用于水处理的聚羟基硫酸氯硅酸盐胶凝剂的制备方法及其制备的胶凝剂
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摘要
PURPOSE: To provide a cohesive agent, which shows stability and good cohesive capacity at a basicity of not less than 70%, and a method for preparing the cohesive agent. CONSTITUTION: The method comprises the steps of (a) mixing 15-28 wt.% of Al(OH)3 having Al2O3 concentration of 40-68%, 50-75 wt.% of HCl at a concentration of 25-35%, 0.5-10 wt.% of H2SO4 at a concentration of 50-98%, and 0.6-25 wt.% of water; (b) reacting the mixture obtained from the step (a) at a temperature of 90-125 deg.C for 5-20 hours to prepare AlClSO3 having Al2O3 concentration of 9-14% and basicity of not more than 10%; (c) mixing 46-75 wt.% of AlClSO3 obtained from the step (b), 10-25 wt.% of NaOH having Na2O concentration of 15-40%, 0.01-10.0 wt.% of Na2SiO3 having SiO2 concentration of 5-40%, and 15-35 wt.% of water; and (d) reacting the mixture obtained from the step (c) at a temperature of 30-60 deg.c with velocity gradient of 1.000 second to prepare Al2(OH)3Cl2(SO4)2(SiO2).
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