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A manufacturing process of Fe/Carbide and Fe/Nitride nano composite powder by Chemical Vapor Condensation

机译:化学气相冷凝法制备铁/碳化物和铁/氮化物纳米复合粉的工艺

摘要

The present invention is a nano-iron by chemical vapor condensation method / carbide and iron / nitride composite powder synthesis process It relates. Nano-iron / iron carbide and / nitride compound Synthesis process according to the chemical vapor condensation method of the present invention, vaporization of vaporizing organic material 140 containing the iron phase with, the organic material 140 and the injection vaporized in the vaporizing which reaction step the carrier gas 160 to react with, and comprises a collecting step of collecting the condensed reaction process 340 generated in the reaction step, the organic material 140 in the gasification step, iron penta carbonyl Neil (Fe (CO) 5 ), ethoxide iron (Fe (OCH 2 CH 3 ) 3 ), iron acetate DE ((CH 3 CO 2 ) 2 Fe) is any one of, the carrier gas in the reaction stage 160 is argon (Ar), carbon monoxide (CO), methane (CH 4 ), ethanol (C 2 H 4 ) is at least one or more of the carrier gas in the reaction step (160) is nitrogen (N 2 ), ammonia (NH 3 ) and is characterized by any one of a mixed gas of these with argon (Ar). According to the present invention, there is produced a complex with the possible benefits of the various nano-iron has a size / nano-iron carbide and / nitride composite powder.
机译:本发明是一种通过化学气相冷凝法制备的纳米铁/碳化物与铁/氮化物复合粉末的合成方法。纳米铁/碳化铁和/氮化物化合物的合成方法根据本发明的化学气相冷凝法,将包含铁相的有机材料140的汽化与其中的有机材料140和注入物汽化,在该反应步骤中进行汽化载气160与之反应,并包括收集步骤,该步骤收集在反应步骤中产生的冷凝反应过程340,气化步骤中的有机材料140,五羰基铁镍(Fe(CO) 5 ),乙醇铁(Fe(OCH 2 CH 3 3 ),乙酸铁DE((CH 3 CO 2 2 Fe)为以下任一种,反应阶段160中的载气为氩气(Ar),一氧化碳(CO),甲烷(CH 4 ),乙醇(C 2 H 4 )是反应步骤(160)中至少一种或多种载气是氮气(N 2 ),氨水(NH 3 ),其特征在于它们与氩气(Ar)的混合气体中的任何一种。根据本发明,制得了具有可能的益处的复合物,其具有各种纳米铁粉的尺寸/纳米碳化铁和/氮化铁复合粉。

著录项

  • 公开/公告号KR100557873B1

    专利类型

  • 公开/公告日2006-03-10

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20040029635

  • 发明设计人 김병기;최철진;김진천;

    申请日2004-04-28

  • 分类号B22F9/28;

  • 国家 KR

  • 入库时间 2022-08-21 21:24:10

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