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Continuous Production Method of 1,2,4-Butanetriol

机译:1,2,4-丁三醇的连续生产方法

摘要

The present invention relates to a continuous method of producing 1,2,4- butane triol , at least 3 nickel catalyst is supplied to the liquid mixture consisting of 2,3- epoxy -1,4- butanediol , and a solvent in a fixed bed continuous reaction system is filled with a metal surface area of / g, reaction in the temperature 10~250 under a hydrogen gas atmosphere , 5 to 300 atm and a reaction pressure of 0.1~30 hr -1 continuously hydrogenolysis under the reaction conditions of the weight space velocity (LHSV) of the step characterized in that it comprises a to carry out the reaction . The present invention is high in productivity over the prior art , environmentally friendly, has the advantage that can be produced in a cost-effective way to come 1,2,4 butanetricarboxylic .
机译:本发明涉及一种生产1,2,4-丁烷三醇的连续方法,将至少3种镍催化剂供给到由2,3-环氧-1,4-丁二醇和溶剂固定的液体混合物中床连续反应系统中填充金属表面积为/ g,在氢气气氛下,5至300 atm的温度和10至250的温度,0.1至30小时的反应压力下进行反应[Sup> -1 在反应条件下连续氢解的重空速(LHSV)步骤的特征在于,它包括进行反应的步骤。与现有技术相比,本发明的生产率高,对环境友好,具有可以以成本有效的方式生产1,2,4-丁三羧酸的优点。

著录项

  • 公开/公告号KR100718767B1

    专利类型

  • 公开/公告日2007-05-16

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20030096499

  • 发明设计人 김태윤;김진웅;이상일;곽병성;

    申请日2003-12-24

  • 分类号C07C29/132;

  • 国家 KR

  • 入库时间 2022-08-21 20:32:11

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