首页> 外国专利> AN IMPROVED PROCESS FOR THE PREPARATION OF SURFACE MODIFIED ZINC OXIDE SENSOR MATERIAL USEFUL FOR SENSING AMMONIA GAS

AN IMPROVED PROCESS FOR THE PREPARATION OF SURFACE MODIFIED ZINC OXIDE SENSOR MATERIAL USEFUL FOR SENSING AMMONIA GAS

机译:一种用于氨气传感的表面改性氧化锌传感器材料的制备方法的改进

摘要

A process for the preparation of surface modified zinc oxide sensor material useful for sensing ammonia gas, which comprises of thoroughly mixing zinc oxide with a binder such as herein described, in presence of solvent such as herein described, drying the resultant mixture for 1-2 hours, compacting the dried powder under pressure of 5 to 10 tons, to obtain zinc oxide pellets, calcining the pellets so obtained at a temperature ranging between 500°C to 1QOO°C for a period of 5 to 16 hours, gradually reducing the temperature at the rate of l°C/min. to 3°C/min. to room temperature, immersing the pellets in a dilute solutions of a ruthenium such as herein described, for a period[ranging between 10 minutes and 15 hours, drying the pellets to incorporate 0.1-3 them heating the resultant pellets at a temperature ranging between 200 and 500 C for a period of 0.5 to 16 hours, to obtain the surface modified zine oxide
机译:一种用于感测氨气的表面改性的氧化锌传感器材料的制备方法,该方法包括在例如本文所述的溶剂存在下,将氧化锌与例如本文所述的粘合剂充分混合,将所得混合物干燥1-2分钟。小时,在5-10吨的压力下将干燥的粉末压实,以获得氧化锌粒料,将如此获得的粒料在500℃至1000℃的温度范围内煅烧5-16小时,逐渐降低温度。以1°C / min的速率。至3°C / min。到室温,将粒料浸入如本文所述的钌的稀溶液中,持续10分钟至15小时,干燥粒料以掺入0.1-3粒,将所得粒料在200至200℃的温度下加热。在500℃下加热0.5-16小时,得到表面改性的氧化锌

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