首页> 外国专利> METHOD FOR THE PREPARATION OF SIZE AND DENSITY CONTROLLED METAL NANOPARTICLE CATALYSTS FOR CARBON NANOTUBE AND METAL NANOPARTICLE CATALYSTS PREPARED BY THE SAME

METHOD FOR THE PREPARATION OF SIZE AND DENSITY CONTROLLED METAL NANOPARTICLE CATALYSTS FOR CARBON NANOTUBE AND METAL NANOPARTICLE CATALYSTS PREPARED BY THE SAME

机译:碳纳米管的尺寸和密度可控的金属纳米催化剂的制备方法及用该方法制备的金属纳米催化剂

摘要

A method for forming catalyst particles with uniform and controlled density and size in a simple manner as compared with conventional methods is provided, and a method for forming nickel nanoparticles with uniform size and density on a substrate of metal or glass using an electroless nickel plating solution is provided. A preparation method of a metal nanoparticle catalyst for forming carbon nanotubes comprises the steps of: (i) cleaning a substrate or a substrate having a film formed thereon and heating the cleaned substrate to a temperature of 55 to 95 deg.C; (ii) spraying an electroless plating solution onto the heated substrate; (iii) spraying a catalyst onto the electroless plating solution-sprayed substrate; and (iv) cleaning and drying the catalyst-sprayed substrate. A preparation method of a metal nanoparticle catalyst for forming carbon nanotubes comprises the steps of: (i) cleaning a substrate or a substrate having a film formed thereon; (ii) spraying an electroless plating solution heated to a temperature of 55 to 95 deg.C onto the cleaned substrate; (iii) spraying a catalyst onto the electroless plating solution-sprayed substrate; and (iv) cleaning and drying the catalyst-sprayed substrate. Further, the electroless plating solution is selected from Ni, Fe, Co and an alloy thereof.
机译:提供了一种与常规方法相比以简单的方式形成具有均匀且受控的密度和尺寸的催化剂颗粒的方法,以及使用化学镀镍溶液在金属或玻璃基板上形成具有均匀尺寸和密度的镍纳米颗粒的方法。提供。用于形成碳纳米管的金属纳米颗粒催化剂的制备方法包括以下步骤:(i)清洁基材或在其上形成有膜的基材,并将清洁后的基材加热至55至95℃的温度; (ii)将化学镀溶液喷涂到加热的基板上; (iii)将催化剂喷涂到喷涂了化学镀溶液的基板上; (iv)清洗并干燥喷有催化剂的基材。用于形成碳纳米管的金属纳米颗粒催化剂的制备方法包括以下步骤:(i)清洁基底或在其上形成有膜的基底; (ii)将加热到55至95℃的化学镀液喷涂到清洁的基板上; (iii)将催化剂喷涂到喷涂了化学镀溶液的基板上; (iv)清洗并干燥喷有催化剂的基材。此外,化学镀溶液选自Ni,Fe,Co及其合金。

著录项

  • 公开/公告号KR20080081630A

    专利类型

  • 公开/公告日2008-09-10

    原文格式PDF

  • 申请/专利权人 KOREA INSTITUTE OF INDUSTRIAL TECHNOLOGY;

    申请/专利号KR20070021930

  • 发明设计人 LEE HONG KEE;LEE HO YOUNG;

    申请日2007-03-06

  • 分类号B01J37/02;B01J23/44;B82B3;

  • 国家 KR

  • 入库时间 2022-08-21 19:53:02

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