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SOLVENT FEEDER, REAGENT BOTTLE, SOLVENT, AND SOLVENT SUPPLY METHOD FOR LIQUID CHROMATOGRAPH MASS SPECTROMETER

机译:液相色谱质谱仪的溶剂进料器,试剂瓶,溶剂和溶剂供应方法

摘要

PROBLEM TO BE SOLVED: To provide a technology for preventing a degradation of analytical sensitivity attributable to chemical noise or degradation of ionization efficiency due to trace substances mixed in a solvent or existing in a laboratory environment in an analysis of protein and so on, using LC-MS.;SOLUTION: A solvent feeder 1 for a liquid chromatograph mass spectrometer includes a suction nozzle 13 inserted into a reagent bottle 2 through a metallic foil sealing a mouth thereof to suck in a solvent, the reagent bottle 2 accommodating the solvent used as a mobile phase of the liquid chromatograph mass spectrometer, a vacuum cap 14 abutted against the mouth of the reagent bottle 2 to cover the mouth and having a pierced hole through which the suction nozzle 13 to be inserted into the reagent bottle 2 is inserted, and a vacuum pump connected to this vacuum cap 14 to suck in air from a space formed between the vacuum cap 14 covering the mouth of the reagent bottle 2 and the metallic foil.;COPYRIGHT: (C)2010,JPO&INPIT
机译:要解决的问题:提供一种技术,该技术可防止由于化学噪声引起的分析灵敏度下降或由于溶剂中混合的微量物质或实验室环境中存在的蛋白质分析等中的微量物质引起的电离效率下降。解决方案:一种用于液相色谱质谱仪的溶剂进料器1,包括一个吸嘴13,该吸嘴13通过密封口的金属箔插入试剂瓶2中,以吸入溶剂,试剂瓶2容纳了用作溶剂的溶剂。在液相色谱质谱仪的流动相中,真空帽14紧靠试剂瓶2的嘴以覆盖该嘴并具有穿孔,要插入到试剂瓶2中的吸嘴13穿过该穿孔。真空泵连接到该真空盖14,以从覆盖试剂瓶2的口的真空盖14和金属容器之间形成的空间吸入空气。箔。;版权所有:(C)2010,JPO&INPIT

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