首页> 外国专利> METHOD FOR MANUFACTURING ULTRAFINE TUNGSTEN CARBIDE POWDER USING MOLTEN SALT-ASSISTED SHS, CAPABLE OF MANUFACTURING ULTRAFINE TUNGSTEN CARBIDE POWDER WITH SELF-PROPAGATING COMBUSTION REACTION

METHOD FOR MANUFACTURING ULTRAFINE TUNGSTEN CARBIDE POWDER USING MOLTEN SALT-ASSISTED SHS, CAPABLE OF MANUFACTURING ULTRAFINE TUNGSTEN CARBIDE POWDER WITH SELF-PROPAGATING COMBUSTION REACTION

机译:利用熔融盐辅助SHS制造超细碳化钨粉的方法,能够通过自蔓延燃烧反应制造超细碳化钨粉

摘要

PURPOSE: A method for manufacturing ultrafine tungsten carbide powder using molten salt-assisted SHS is provided to control particles size of the powder with a sub-micron unit, and to produce the powder of high purity.;CONSTITUTION: A method for manufacturing ultrafine tungsten carbide powder using molten salt-assisted SHS includes the following steps of: gaining a raw material by mixing organic materials containing oxygen and carbon, tungsten oxide, a reducing agent, a carbon source, alkaline salt, carbonate and a reaction activator; putting the raw material to a high pressure container; reducing the tungsten oxide by igniting and heating the raw material locally; washing a generated reaction product with distilled water; and washing the product with an acid solution. The alkaline salt is LiF, LiCl, LiBr, LiI, NaF, NaCl, NaBr, NaI, KF, KCl, KBr, KI, or their salt mixture. The reaction activator includes sodium carbonate, potassium carbonate, sodium hydrogen carbonate, potassium hydrogen carbonate, magnesium carbonate, calcium carbonate, ammonium carbonate, urea, melamine, polystyrene, and their mixture.;COPYRIGHT KIPO 2010
机译:目的:提供一种使用熔融盐辅助SHS制造超细碳化钨粉末的方法,以亚微米单位控制粉末的粒度,并生产高纯度的粉末。;组成:一种制造超细钨的方法使用熔融盐辅助SHS制成的碳化物粉末包括以下步骤:通过混合含氧和碳的有机材料,氧化钨,还原剂,碳源,碱金属盐,碳酸盐和反应活化剂来获得原料。将原料放入高压容器中;通过局部点燃和加热原料来减少氧化钨;用蒸馏水洗涤生成的反应产物;并用酸溶液洗涤产品。碱性盐是LiF,LiCl,LiBr,LiI,NaF,NaCl,NaBr,NaI,KF,KCl,KBr,KI或它们的盐混合物。反应活化剂包括碳酸钠,碳酸钾,碳酸氢钠,碳酸氢钾,碳酸镁,碳酸钙,碳酸铵,尿素,三聚氰胺,聚苯乙烯及其混合物。COPYRIGHTKIPO 2010

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