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Rapid Identification of Explosives Using Thin-Layer Chromatography and Colorimetric Techniques

机译:薄层色谱和比色技术快速鉴定炸药

摘要

A thin-layer chromatography method for identifying material present in a sample on a location including the steps of provide a thin-layer chromatography plate, wetting a swab is with a solvent providing a wetted swab, contacted the location of interest is with the wetted swab to obtain the sample providing a wetted swab with sample, placing the wetted swab with sample in the solvent to dissolve the sample and provide a solvent with sample, dipping a micropipette into the solvent with sample to obtain an amount of the solvent with sample, spotting the amount of the solvent with sample on the thin-layer chromatography plate, allowed the amount of the solvent with sample on the thin-layer chromatography plate to dry providing a thin-layer chromatography plate with sample, placing the a thin-layer chromatography plate with sample into a developing chamber with solvent mixture, allowing the thin-layer chromatography plate with sample to develop producing a developed thin-layer chromatography plate with sample, removing the developed thin-layer chromatography plate with sample from the developing chamber, and illuminating the developed thin-layer chromatography plate with sample with ultra violet light to produce an image for identifying the material present in the sample.
机译:一种薄层色谱法,用于识别位置上样品中的物质,包括以下步骤:提供薄层色谱板,用溶剂润湿拭子以提供润湿的拭子,将感兴趣的位置与润湿的拭子接触要获得提供带有样品的拭子的样品,请将带有样品的拭子放入溶剂中以溶解样品并提供带有样品的溶剂,将微量移液器浸入带有样品的溶剂中以获得一定量的带有样品的溶剂,点样量的薄层色谱板上的样品中溶剂的量,使薄层色谱板上的样品中溶剂的量干燥,以提供具有样品的薄层色谱板,并放置薄层色谱板将样品加入到带有溶剂混合物的显影室中,使带有样品的薄层色谱板显影,生成显影的薄层色谱仪y将带有样品的板,从显影室中取出带有样品的显影的薄层色谱板,并用紫外线照射带有样品的显影的薄层色谱板以产生图像,以鉴定样品中存在的物质。

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