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Thin-Layer Chromatography and Colorimetric Analysis of Multi-Component Explosive Mixtures

机译:多组分炸药混合物的薄层色谱和比色分析

摘要

A thin-layer chromatography method for detection and identification of common military and peroxide explosives in samples includes the steps of provide a reverse-phase thin-layer chromatography plate; prepare the plate by marking spots on which to deposit the samples by touching the plate with a marker; spot one micro liter of a first standard onto one of the spots, spot one micro liter of a second standard onto another of the spots, and spot samples onto other of spots producing a spotted plate; add eluent to a developing chamber; add the spotted plate to the developing chamber; remove the spotted plate from the developing chamber producing a developed plate; place the developed plate in an ultraviolet light box; add a visualization agent to a dip tank; dip the developed plate in the dip tank and remove the developed plate quickly; and detect explosives by viewing said developed plate.
机译:一种用于检测和鉴定样品中常见军用和过氧化物炸药的薄层色谱法,包括以下步骤:提供反相薄层色谱板;通过用记号笔接触标板,在标有待沉积样品的点上进行标记来制备标板;将一个微升的第一标准液点到一个斑点上,将一个微升的第二标准液点到另一个斑点上,并将样品点到另一个斑点上,从而产生一个斑点板;向显影室添加洗脱液;将斑点板添加到显影室中;从显影室中除去斑点板,产生显影板;将显影后的板放入紫外线灯箱中;向浸渍罐添加可视化代理;将已显影的板浸入浸液罐中并快速取出已显影的板;并通过查看所述显影板来检测爆炸物。

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