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Process for the simultaneous and selective preparation of single-walled and multi-walled carbon nanotubes

机译:同时选择性制备单壁和多壁碳纳米管的方法

摘要

Processes for the simultaneous and selective growth of single walled and multiwalled carbon nanotubes in a single set of experiments are disclosed. The processes may include preparing a graphite electrode rod containing catalyst selected from Fe, Co, Ni, and a mixture thereof, acting as an anode. The process may include preparing another graphite electrode rod, each electrode having a distal and a proximal end. The process may include placing the above said two electrodes parallel to each other and their axis being substantially aligned in a chamber. The process may further include creating a DC-arc discharge inside the chamber by applying a DC-current voltage. The process may further include an cooling assembly having a cooling coil that surrounds the two electrodes. The cooling assembly may be used to maintain a temperature gradient that permits the depositing of single walled and multiwalled carbon nanotubes simultaneously in one experiment.
机译:公开了在单组实验中同时且选择性地生长单壁和多壁碳纳米管的方法。所述方法可包括制备充当阳极的,包含选自Fe,Co,Ni及其混合物的催化剂的石墨电极棒。该方法可以包括准备另一石墨电极棒,每个石墨电极棒具有远端和近端。该过程可以包括将上述两个电极彼此平行放置,并且其轴线在腔室中基本对准。该过程可以进一步包括通过施加直流电流电压在腔室内产生直流电弧放电。该方法可以进一步包括冷却组件,该冷却组件具有围绕两个电极的冷却盘管。冷却组件可用于维持温度梯度,该温度梯度允许在一个实验中同时沉积单壁和多壁碳纳米管。

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