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IDENTIFICATION METHOD OF FULLERENES C60 AND C70 IN STEELS AND CAST IRONS

机译:钢铁和铸离子中富勒烯C 60 和C 70 的鉴定方法

摘要

FIELD: measurement equipment.;SUBSTANCE: invention refers to the procedure of determining fullerenes C60 and C70 in iron-carbon steels. Metal sample of iron-carbon alloy is crushed and treated with hydrofluoric acid. The formed deposit is filtered, dried and crushed. The obtained fine powder is mixed with potassium bromide powder. The obtained mixture is added to the pill and identification of fullerenes is performed on IR Fourier spectrometre. The obtained spectra are decoded according to reference spectra of C60 and C70 fullerenes.;EFFECT: invention allows improving efficiency and sensitivity of the method for determining fullerenes included in the composition of steels and cast irons.
机译:技术领域:本发明涉及确定铁碳钢中富勒烯C 60 和C 70 的程序。将铁-碳合金的金属样品压碎并用氢氟酸处理。将形成的沉积物过滤,干燥并压碎。将获得的细粉与溴化钾粉混合。将获得的混合物加入药丸中,并在红外傅里叶光谱仪上进行富勒烯的鉴定。根据C 60 和C 70 富勒烯的参考光谱对获得的光谱进行解码。效果:本发明可以提高测定组合物中所含富勒烯的方法的效率和灵敏度。钢和铸铁。

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