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Hydrothermal reaction visible for the cell to be used in the hydrothermal reaction visible method and the method of the microwave

机译:水热反应可见法和微波法中所用电池的水热反应可见

摘要

PROBLEM TO BE SOLVED: To provide a new microwave hydrothermal reaction visualizing cell for confirming visually by a microwave, a change of a superheated state to aqueous solution stored in a cell and a change generated when cooling the solution.;SOLUTION: The hydrothermal reaction visualizing cell by the microwave is constituted as follows: a transparent pressure-resistant glass tube 2 for observation is stored concentrically inside a transparent cylinder 1; an exhaust pump 16 is connected through a suction tube 14 to a space part A formed between both of the transparent cylinder 1 and the glass tube 2 for observation; a cooling water storage tank 17 is connected through a water supply tube 15, to thereby constitute the space A as a space for forming a vacuum heat insulating layer when raising a temperature or as a space for introducing cooling water during a cooling period; further, an introduction pipe 5 for introducing a solution which is an observation object is connected to the glass tube 2 for observation; and the transparent cylinder 1 and the glass tube 2 for observation having such a configuration are set in a heating chamber 18 by the microwave with an openable/closable door having a transparent window.;COPYRIGHT: (C)2009,JPO&INPIT
机译:要解决的问题:提供一种新的微波水热反应可视化池,用于通过微波目视确认,过热状态向存储在池中的水溶液的变化以及冷却溶液时产生的变化。由微波构成的单元如下构成:将观察用的透明耐压玻璃管2同心地收纳在透明圆筒1的内部。排气泵16通过吸入管14连接到形成在透明圆筒1和玻璃管2之间的用于观察的空间部分A。冷却水储罐17通过供水管15连接,从而将空间A构成为当温度升高时用于形成真空绝热层的空间或作为在冷却期间引入冷却水的空间。另外,在观察用玻璃管2上连接有用于引入作为观察对象的溶液的引入管5。具有这种结构的透明圆筒1和观察用玻璃管2通过具有可开闭的具有透明窗的门的微波而被设置在加热室18内。版权所有:(C)2009,JPO&INPIT

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