首页> 外国专利> Hydrogen halide formed is continuously removed from the organic solvent, halogenated Rirenkarubon acid imide by a halogen element in a two-phase mixture comprising an organic solvent and water

Hydrogen halide formed is continuously removed from the organic solvent, halogenated Rirenkarubon acid imide by a halogen element in a two-phase mixture comprising an organic solvent and water

机译:在包含有机溶剂和水的两相混合物中,通过卤素元素将形成的卤化氢连续地从卤素卤化的Rirenkarubon酰亚胺的有机溶剂中除去。

摘要

General formula I [wherein, have the following meanings variables: A, of B, when n or imide group is 1 taken together, B and A is 1 or is Hal both It is hydrogen, independently of one another R, R 1 is; which is a hydrogen group and the other and a and Hal group number: hetaryl alkyl, cycloalkyl, aryl or optionally substituted; are Hal, chlorine, bromine aralkyl or iodine; are n, is 1, 2 or 3; wherein, x is, 'B' and group A of the general formula II Rirenkarubon acid imides are halogenated] 2 to 8, and when n or an imide group together is 1, both produced by reacting in the presence of an organic solvent L1 inert and halogen element and Rirenkarubon acid imide] is hydrogen A method for, is characterized in that continuously withdrawing the hydrogen halide formed during the reaction from the solvent L1, preparation of Rirenkarubon acid imides are halogenated of the general formula I.
机译:通式I [其中,具有以下含义变量:B的A,当n或酰亚胺基为1时,B和A为1或均为Hal均为氢,彼此独立地为R,R 1 是;其中一个是氢基,另一个是和Hal基团数:杂芳基烷基,环烷基,芳基或任选取代的;是Hal,氯,溴芳烷基或碘;是n,是1、2或3;其中,x为'B',通式II的基团A Rirenkarubon酰亚胺被卤代] 2至8,并且当n或酰亚胺基一起为1时,两者都是通过在惰性有机溶剂L1的存在下反应制备的一种卤素的方法,其特征在于,从溶剂L1中连续抽出反应过程中形成的卤化氢,制备通式I的卤代雷卡鲁酮酰亚胺。

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