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Method of controlling a process of acetic acid

机译:控制乙酸过程的方法

摘要

A method of controlling a process for producing acetic acid by carbonylation of methanol or carbonylatable aderived thereof, comprising the steps of: monitoring the production rate of acetic acid; reduce the production rate in response to uncambio in operating conditions outside the normal operating range of a; after reducing lavelocidad production, control the process to reduced production rate; and increase production velocidadde after boarding the change in operating conditions until at least lavelocidad production again said normal operating range; wherein for at least one of lospasos to slow production, control the process to reduced production rate, yaumentar production speed until the production rate again said operativonormal interval, the process is controlled by multivariable control not linear based on a process model, endonde process control is during the change and / or during a recovery period programs after approached the change and where the change in operating conditions a alteraciónsignificativa the selected process group should that consisting of: (a) a substantial reduction in ladisponibilidad carbon monoxide; (B) failure of a pump catalyst; (C) loss of cooling capacity or decalentamiento; (D) flooding a subsequent purification column; (E) desviacionessignificativas of expected compositions in one or more streams associated with depurificación column; (F) a lack of storage capacity for acetic acid product; and combinations thereof delas.
机译:控制通过甲醇或其衍生的羰基的羰基化生产乙酸的方法的方法,包括以下步骤:监测乙酸的产生速率;在正常工作范围a以外的工作条件下,响应uncambio降低生产率;减少拉韦罗达生产后,控制工艺以降低生产率;并在改变运行条件之后提高生产速度,直到至少拉维达生产再次达到正常运行范围为止;其中对于罗帕索斯中的至少一个以减慢生产速度,将过程控制为降低生产率,以无休止的生产速度直到生产率再次达到操作正常区间而言,通过基于过程模型的非线性多变量控制来控制过程,内在过程控制是在变更期间和/或恢复期间,在接近变更之后的程序中,以及在操作条件发生变更的情况下,选定的过程组应包括以下内容:(a)大大减少拉索尼比德一氧化碳; (B)泵催化剂失灵; (C)冷却能力降低或失去十足的作用; (D)注入后续的纯化塔; (E)与去纯化柱相关的一种或多种物流中预期成分的脱维亚度; (F)乙酸产品的储存能力不足;及其组合delas。

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