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TOTAL PHOSPHOROUS QUANTITY DETERMINATION METHOD

机译:总磷量的测定方法

摘要

The disclosed method determines the total phosphorous quantity in test water safely and in a short time period by breaking down phosphorous compounds included in test water and converting to phosphate ions, and then determining the quantity of phosphate ions in the test water. In the method, first sulfuric acid and alkali metal salts of peroxodisulfuric acid are added to test water, and the mixture is heated for a prescribed time period at a temperature from 65˚C to boiling temperature. A colour former formed from an aqueous solution is added to the test water, said aqueous solution containing at least one hydroxyl group-containing compound selected from the hydroxyl group-containing compound group consisting of hydroxyl carboxylic acids and alditol, a vanadium compound having a vanadium valence of 3-5, a non-reducing oligosaccharide capable of generating a 5 carbon aldose, a 6 carbon aldose or a 6 carbon ketose by means of decomposition, and a 7-molybdic acid 6-ammonium, and after heating the test water to at least 65˚C for a prescribed time period, the light absorbance of the test water for an arbitrary wavelength occurring in the range of 600-950nm is measured.
机译:通过分解包括在测试水中的磷化合物并转化为磷酸根离子,然后确定测试水中的磷酸根离子的量,所公开的方法在短时间内安全地确定测试水中的总磷含量。在该方法中,首先将过硫酸和过氧二硫酸的碱金属盐添加到测试水中,并将混合物在65°C至沸点的温度下加热规定的时间。将由水溶液形成的成色剂添加到测试水中,所述水溶液包含至少一种选自羟基羧酸的化合物,所述羟基化合物包括由羟基羧酸和醛糖醇组成的含羟基化合物,具有钒的钒化合物。化合价为3-5,能够通过分解生成5碳醛糖,6碳醛糖或6碳酮糖的非还原性寡糖和7钼酸6-铵,然后将测试水加热至在规定时间至少65°C的条件下,测量测试水在600-950nm范围内出现的任意波长的吸光度。

著录项

  • 公开/公告号WO2012014346A1

    专利类型

  • 公开/公告日2012-02-02

    原文格式PDF

  • 申请/专利权人 MIURA CO. LTD.;ISHII HIROSHI;

    申请/专利号WO2011JP00460

  • 发明设计人 ISHII HIROSHI;

    申请日2011-01-28

  • 分类号G01N31/00;G01N33/18;

  • 国家 WO

  • 入库时间 2022-08-21 17:18:01

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