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Synthesis of SiC powder with carbon deposition on the silicon powder

机译:碳粉沉积在硅粉上合成SiC粉

摘要

The present invention comprises the steps of (a) selecting a high purity silicon powder; (b) distilling the hydrocarbon compound one or more times; (c) immersing the hydrocarbon in silicon powder in a tubular furnace at 800-1200 ° C. for 0.5-3 hours; (d) heat-treating the carbon powder deposited silicon powder to react with silicon carbide; And (e) heating in the presence of air to remove excess carbon. The reaction is completed when the temperature is increased by depositing carbon on the high purity silicon powder through the heat treatment process only with high purity hydrocarbon. Since it is possible to synthesize high-purity silicon carbide by adjusting the heating temperature while injecting air thereafter, the problem that the yield is reduced or the greenhouse gas is generated by the silicon monoxide and carbon monoxide generated when using silica and carbon as a raw material. Conventional silicon carbide, such as the problem of non-homogeneity generated when carbon black is mixed with silicon powder and the limitation of purity of carbon black, and the use of a binder to mix silicon powder and carbon black. The present invention provides a method for synthesizing silicon carbide with carbon deposition on silicon powder that can solve the problems of yield reduction, environmental problems, and inhomogeneity accompanying mixing.
机译:本发明包括以下步骤:(a)选择高纯度硅粉; (b)将烃化合物蒸馏一次或多次; (c)将碳氢化合物浸入硅粉中,在管式炉中于800-1200℃下浸0.5-3小时; (d)热处理碳粉沉积的硅粉,使其与碳化硅反应; (e)在空气中加热以除去多余的碳。当仅通过使用高纯度烃通过热处理过程将碳沉积在高纯度硅粉上来提高温度时,反应就完成了。由于可以通过在随后注入空气的同时调节加热温度来合成高纯度碳化硅,因此存在产量降低或由于使用二氧化硅和碳作为原料而产生的一氧化硅和一氧化碳产生温室气体的问题。材料。常规的碳化硅,例如当将炭黑与硅粉混合时会产生不均匀性的问题,以及炭黑纯度的限制,以及使用粘合剂将硅粉和炭黑混合的问题。本发明提供了一种用于在碳化硅粉末上沉积碳的碳化硅的合成方法,该方法可以解决产率降低,环境问题以及伴随混合的不均匀性的问题。

著录项

  • 公开/公告号KR101151299B1

    专利类型

  • 公开/公告日2012-06-08

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20100072833

  • 申请日2010-07-28

  • 分类号C01B31/36;C04B35/565;

  • 国家 KR

  • 入库时间 2022-08-21 17:07:58

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