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METHOD OF DETERMINING DEGREE OF DEACETYLATION OF CHITOSAN
METHOD OF DETERMINING DEGREE OF DEACETYLATION OF CHITOSAN
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机译:测定壳聚糖脱乙酰度的方法
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摘要
FIELD: chemistry.;SUBSTANCE: method involves taking a certain weighed amount of chitosanium chromate which is first purified from extraneous impurities and reduced to constant weight. The weighed amount is then turned into a stable weighted form through thermal treatment on air at temperature 800-900°C to form chromium oxide Cr2O3. The weight of the formed chromium oxide is then determined. Content of chromic acid in the initial weighed amount of chitosanium chromate is then calculated from the weight of chromium oxide. The degree of deacetylation of chitosan is calculated using defined formulae.;EFFECT: invention enables to increase accuracy of determining degree of deacetylation of chitosan.;2 ex
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机译:领域:化学;物质:该方法涉及取一定量的铬酸壳聚糖,首先从外来杂质中纯化并还原至恒重。然后通过在800-900℃的温度下在空气中热处理将称量的量变成稳定的称量形式,以形成氧化铬Cr 2 Sub> O 3 Sub>。然后确定所形成的氧化铬的重量。然后从氧化铬的重量中计算出最初称量的铬酸壳聚糖铬中铬酸的含量。壳聚糖的脱乙酰基度使用定义的公式计算;效果:本发明能够提高确定壳聚糖的脱乙酰基度的准确性。
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