首页> 外国专利> PROCESS FOR OBTAINING BORAZANE, SUITABLE FOR OBTAINING BORAZANE DE GRANDE, OR VERY HIGH PURITY; BORAZANE OF VERY LARGE PURITY

PROCESS FOR OBTAINING BORAZANE, SUITABLE FOR OBTAINING BORAZANE DE GRANDE, OR VERY HIGH PURITY; BORAZANE OF VERY LARGE PURITY

机译:获得硼氮烷的过程,适合获得硼砂烷的过程或非常高的纯度;硼砂非常大的纯度

摘要

The present invention relates to a method for obtaining borazane, said method being suitable for obtaining borazane containing a low level of impurities. The borazane (obtained by reaction of at least one ammonium salt with at least one alkali and/or alkaline earth metal borohydride) in solution in THF is selectively precipitated with a non-solvent. The precipitated borazane can further be purified by selective dissolution. The borazane obtained after selective precipitation and dissolution contains less than 1% by weight of impurities and/or does not exhibit exothermic decomposition in the solid state with a temperature range of the endothermic melting peak above 110° C.
机译:本发明涉及一种获得硼烷的方法,该方法适合于获得含有少量杂质的硼烷。用非溶剂选择性地沉淀在THF溶液中的硼烷(通过至少一种铵盐与至少一种碱金属和/或碱土金属硼氢化物反应获得)。沉淀的硼氮烷可通过选择性溶解进一步纯化。在选择性沉淀和溶解后获得的硼烷具有小于1重量%的杂质和/或在吸热熔融峰的温度范围高于110°C时不表现出固态的放热分解。

著录项

  • 公开/公告号FR2960230B1

    专利类型

  • 公开/公告日2012-08-17

    原文格式PDF

  • 申请/专利权人 SNPE MATERIAUX ENERGETIQUES;

    申请/专利号FR20100053990

  • 发明设计人 JEAN-PHILIPPE GOUDON;JOEL RENOUARD;

    申请日2010-05-21

  • 分类号C01B35/14;

  • 国家 FR

  • 入库时间 2022-08-21 17:04:14

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号