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METHOD FOR MANUFACTURING POROUS SILICA-CONTAINING PARTICLE, POROUS SILICA, AND POROUS SILICA CONTAINING PARTICLE

机译:制造多孔含二氧化硅颗粒的方法,多孔二氧化硅和含多孔二氧化硅的颗粒

摘要

PROBLEM TO BE SOLVED: To provide a method for manufacturing satisfactory porous-silica containing particles.SOLUTION: The method for manufacturing satisfactory porous silica-containing particles includes: a process (a) of preparing porous silica; a process (b) of bringing the porous silica into contact with liquid containing a metal or a compound having the metal as an elemental composition, and impregnating the holes of the porous silica with the liquid; and a process (c) of carrying out heat treatment after the process (b), and forming fine particles having the metal or the metal compound in the holes of the porous silica. Also, the porous silica is synthesized by hydrolyzing alkoxysilane with a nonsolvent system so that it is possible to synthesize the porous silica having fine pore diameters. The porous silica is used as a template so that it is possible to easily form even particles (for example, W, Cu, Cr, Mn, Fe, Co or Ni or their metal oxides) showing unprecedented specific quality in the state of bulk.
机译:解决的问题:提供一种制造令人满意的含多孔二氧化硅的颗粒的方法。解决方案:制造令人满意的含多孔二氧化硅的颗粒的方法包括:(a)制备多孔二氧化硅的方法; (b)使多孔质二氧化硅与含有金属或具有该金属作为元素组成的化合物的液体接触,并用该液体浸渍多孔质二氧化硅的孔的工序。工序(c)是在工序(b)之后进行热处理,在多孔二氧化硅的孔中形成具有金属或金属化合物的微粒的工序。另外,通过用非溶剂体系水解烷氧基硅烷来合成多孔二氧化硅,从而可以合成具有细孔径的多孔二氧化硅。多孔二氧化硅被用作模板,使得可以容易地形成均匀的颗粒(例如,W,Cu,Cr,Mn,Fe,Co或Ni或它们的金属氧化物),并且在堆积状态下显示出前所未有的特定质量。

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