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Method of making a submicron cemented carbide powder mixture with low compacting pressure and the resulting powder

机译:压实压力低的亚微米硬质合金粉末混合物的制备方法及所得粉末

摘要

There is disclosed a method of making a ready to press cemented carbide powder with low compaction pressure suitable for the production of submicron cemented carbide by means of powder metallurgical techniques milling, pressing and sintering. The method comprises using from about 1 to about 3 wt-% pressing agent with the following composition, less than about 90 wt-% PEG and from about 10 to about 75 wt-% of blends of high molecular (C12-C20) saturated or unsaturated fatty acids, or salts thereof containing at least one element of Al, Ba, Ca, Co, Cr, Mg, N, Na, V, Zn. Preferably the grain size of the cemented carbide powder is submicron. In a preferred embodiment the method includes a dry pre-milling of the hard constituents mainly WC-powder for about 2-45 hours in ball mills with cemented carbide milling bodies or using other suitable dry milling techniques prior to a wet milling step. The invention also relates to the powder obtained by the method.
机译:公开了一种通过粉末冶金技术研磨,压制和烧结来制备适用于生产亚微米硬质合金的,具有低压实压力的预压硬质合金粉末的方法。该方法包括使用具有以下组成的约1至约3wt%的加压剂,小于约90wt%的PEG和约10至约75wt%的饱和的(C12- <C20)的高分子共混物或包含至少一种元素的不饱和脂肪酸或其盐,所述盐包含Al,Ba,Ca,Co,Cr,Mg,N,Na,V,Zn。优选地,硬质合金粉末的晶粒尺寸为亚微米。在一个优选的实施方案中,该方法包括在具有硬质合金研磨体的球磨机中对硬质成分主要是WC-粉末进行干式预研磨约2-45小时,或者在湿式研磨步骤之前使用其他合适的干式研磨技术。本发明还涉及通过该方法获得的粉末。

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