首页> 外国专利> SYNTHESIS OF 4-TERTBUTYLCALIXNARENES HAVING PHENYL SUBSTITUENT/SUBSTITUTED PHENYL ON METHYLENE BRIDGES.

SYNTHESIS OF 4-TERTBUTYLCALIXNARENES HAVING PHENYL SUBSTITUENT/SUBSTITUTED PHENYL ON METHYLENE BRIDGES.

机译：在亚甲基桥上合成具有苯基取代基/取代苯基的4-叔丁基杯[N]芳烃。

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摘要

The present invention relates to a novel process for preparing 2,8,14,20,26,32,38,44- octa phenyl -5,11,17,23,29, 35, 41, 47 - octa-tert butyl 49,50,51,52,53,54,55,56- octahydroxycalix [8]arene ( XXXI ); 2,8,14,20,26,32-hexa(4-chloro)phenyl-5,l 1,17,23,29, 35 -hexa4ertbutyl-37,38,39,40,41,42-hexahydroxycalix[6]arene (XXXII); 2,8,14,20,26,32- hexa(3-chloro)phenyl-5,l 1,17,23,29, 35 -hexa-tertbutyl-37,38,39,40,41,42- hexahydroxycalix[6]arene (XXXIII); 2,8,14,20,26,32,38,44,50- nona (4-bromo) phenyl- 5,11,17,23,29,35,41,47,53- nona-tertbutyl- 55,56,57,58,59,60,61, 62, 63-nonahydroxycalix [9] arene ( XXXIV}; 2,8,14,20,26,32,38,44- octa (4-fluoro) phenyl -5,11 ,,17,23,29,35,41,47- octa-tertbutyl 49,50,51,52,53,54,55,56- octahydroxycalix [8]arene (XXXV):- 2,8,14,20,26,32,38,44,50,56-deca (4-nitro) phenyl-5,11,17,23,29,35,41,47,53,59-deca- tertbutyl-61,62,63,64, 65,66,67, 68, 69,70- decahydroxycalix [10] arene (XXXVI); 2,8,14,20,26,32,38,44,50,56,- deca (3-nitro) phenyl-5,11,17,23,29,35,41,47,53,59-deca- tertbutyl- 61,62,63,64, 65,66,67, 68, 69,70- decahydroxycalix [10] arene ( XXXVII); 2,8,14,20,26,32,38,44,50,56,- deca (2-nitro) phenyl- 5,11,17,23,29,35,41,47,53,59-deca- tertbutyl- 61,62,63,64,65,66, 67, 68, 69,70- decahydroxycalix [10] arene (XXXVIII); 2,8,14,20,26,32,38,44,50,56-deca (4-cyano)phenyl-5,11,17,23,29,35,41,47,53,59-deca- tertbuty!-61,62,63,64, 65,66,67, 68, 69,70- decahydroxycalix [10] arene ( XXXIX); 2,8,14,20,26,32,38,44- octa (4-methoxy) phenyl -5,11„17,23,29,35,41,47- octa-tertbutyl 49,50,51,52, 53, 54, 55,56- octahydroxycalix [8]arene (XL); 2,8,14,20,26,32,38,44- octa (3- mthoxy) phenyl- 5,11„17,23,29,35,41,47- octa-tertbutyl 49,50,51,52,53, 54,55,56- octahydroxycalix [8]arene (XU); 2,8,14,20,26,32-hexa(3,4-dimethoxy)phenyl- 5,11,17,23,29, 35 -hexa-tertbutyl-37,38,39,40,41,42-hexahydroxycalix[6]arene (XLII); 2,8,14,20- tetra (3,4,5,- trimethoxy) phenyl - 5,11,17,23 tetra-tertbutyl 25,26,27,28-tetrahydroxycalix [4] arene (XLIII); 2,8,14,20- tetra (2,4,6- trimethoxy) phenyl - 5,11,17,23 tefra-terlbutyl 25,26,27,28- telrahydroxycalix [A] arene ( XL1V):- 2,8,14,20- tetra (4-dimethylamino) phenyl - 5,11,17,23 tetra-tertbutyl 25,26,27,28- tetrahydroxycalix [4] arene ( XLV ) in presence of a solvent and a base.

机译：本发明涉及一种制备2,8,14,20,26,32,38,44-辛基苯基-5,11,17,23,29,35,41,47-辛基叔丁基49的新方法，50,51,52,53,54,55,56-八羟基杯[8]芳烃（XXXI）; 2,8,14,20,26,32-六（4-氯）苯基-5,1 1,17,23,29，35-六叔丁基-37,38,39,40,41,42-六羟基杯[6 ]芳烃（XXXII）; 2,8,14,20,26,32-六（3-氯）苯基-5,1 1,17,23,29，35-六叔丁基-37,38,39,40,41,42-六羟基杯[6]芳烃（XXXIII）; 2,8,14,20,26,32,38,44,50-壬基（4-溴）苯基-5,11,17,23,29,35,41,47,53-壬基叔丁基-55， 56,57,58,59,60,61，62，63-九壬基杯[9]芳烃（XXXIV}; 2,8,14,20,26,32,38,44-八（4-氟）苯基-5 ，11 ,, 17,23,29,35,41,47-八叔丁基49,50,51,52,53,54,55,56-八羟基杯[8]芳烃（XXXV）：-2,8,14 ，20,26,32,38,44,50,56-十（4-硝基）苯基-5,11,17,23,29,35,41,47,53,59-十叔丁基-61,62 ，63,64，65,66,67，68，69,70-十羟基杯[10]芳烃（XXXVI）; 2,8,14,20,26,32,38,44,50,56，-十（3 -硝基）苯基-5,11,17,23,29,35,41,47,53,59-叔丁基-61,62,63,64，65,66,67，68，69,70-十羟基杯[10]芳烃（XXXVII）; 2,8,14,20,26,32,38,44,50,56，-十（2-硝基）苯基-5,11,17,23,29,35,41 ，47,53,59-叔丁基-61,62,63,64,65,66，67，68，69,70-十羟基杯[10]芳烃（XXXVIII）; 2,8,14,20,26， 32,38,44,50,56-十（4-氰基）苯基-5,11,17,23,29,35,41,47,53,59-十丁基！-61,62,63,64 ，65,66,67、68、69,70-十羟基杯[10]芳烃（XXXIX）; 2,8,14,20,26,32,38， 44-八（4-甲氧基）苯基-5,11„ 17,23,29,35,41,47-八叔丁基49,50,51,52，53，54，55,56-八羟基杯[8]芳烃（XL）; 2,8,14,20,26,32,38,44-八（3-甲氧基）苯基-5,11„ 17,23,29,35,41,47-八叔丁基49,50,51,52 ，53，54,55,56-八羟基杯[8]芳烃（XU）; 2,8,14,20,26,32-六（3,4-二甲氧基）苯基-5,11,17,23,29，35-六叔丁基-37,38,39,40,41,42-六羟基杯[6]芳烃（XLII）; 2,8,14,20-四（3,4,5，-三甲氧基）苯基-5,11,17,23四叔丁基25,26,27,28-四羟基杯[4]芳烃（XLIII）; 2,8,14,20-四（2,4,6-三甲氧基）苯基-5,11,17,23四叔丁基25,26,27,28-叔羟基杯[A]芳烃（XL1V）：-2， 8,14,20-四（4-二甲基氨基）苯基-5,11,17,23四叔丁基25,26,27,28-四羟基杯[4]芳烃（XLV）在溶剂和碱的存在下。

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公开/公告号IN2010MU03471A

专利类型
公开/公告日2013-06-28

原文格式PDF
申请/专利权人
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申请/专利号IN3471/MUM/2010
发明设计人 SHRIMANT V RATHOD;DR M M V RAMANA;M S RAJE;
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申请日2010-12-21
分类号C07C235/32;C07C37/52;
国家 IN
入库时间 2022-08-21 16:41:26

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