首页> 外国专利> MICROWAVE ENHANCED SYNTHESIS OF 4-TERTBUTYLCALIXNARENES HAVING PHENYL SUBSTITUENT OR SUBSTITUTED PHENYL ON METHYLENE BRIDGES IN PRESENCE OF K2CO3.

MICROWAVE ENHANCED SYNTHESIS OF 4-TERTBUTYLCALIXNARENES HAVING PHENYL SUBSTITUENT OR SUBSTITUTED PHENYL ON METHYLENE BRIDGES IN PRESENCE OF K2CO3.

机译：在存在K2CO3的亚甲基桥上具有苯基取代基或取代苯基的4-叔丁基杯[N]芳烃的微波增强合成。

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摘要

The present invention relates to a novel process for preparing 2,8,14,20,26,32,38,44,50,56,- deca (2-nitro) phenyl- 5,11,17,23,29,35,41,47, 53,59-deca-tertbutyl- 61,62,63,64,65,66, 67, 68, 69,70- decahydroxycalix [10] arene (XVI); 2,8,14,20,26,32,38,44,50,56,- deca (3-nitro) phenyl- 5,11,17,23,29,35,41,47,53,59-deca-tertbutyl- 61,62,63,64,65,66, 67, 68, 69,70- decahydroxycalix [10] arene (XVII); 2,8,14,20,26,32,38,44,50,56-deca(4- nitro)phenyl-5,l 1,17,23,29,35,41,47, 53,59-deca-tertbutyl- 61,62,63,64,65,66,67, 68, 69,70- decahydroxycalix [10] arene (XVIII); 2,8,14,20,26,32,38,44,50,56-deca (4-cyano) phenyl- 5,11,17,23,29,35,41,47,53,59-deca-tertbutyl- 61,62,63,64,65,66,67, 68, 69,70- decahydroxycalix [10]arene (XIX); 2,8,14,20,26,32,38,44- octa (4-fluoro) phenyl -5,11ž17,23,29,35,41,47-octatertbutyl49,50,51,52,53,54,55,56- octahydroxycalix [8]arene (XX); 2,8,14,20,26,32,38,44- octa (4-methoxy) phenyl -5,11,,17,23,29,35,41,47-octa-tertbutyl 49,50,51,52, 54,55,56, octahydroxycalix [8]arene (XXI); 2,8,14,20,26,32,38,44- octa (3-methoxy) phenyl -5,11ž17,23,29,35,41,47- octa-tertbutyl 49,50,51,52,53,54,55,56- octahydroxycalix [8]arene (XXII); 2,8,14,20,26,32,38,44- octa-phenyl -5,11,17,23,29,35,41,47- octa- tertbutyl 49,50,51,52,53,54,55,56- octahydroxycalix [8]arene ( XXIII); 2,8,14,20,26,32-hexa(3-chloro)phenyl-5,l 1,17,23,29, 35 - hexa-tertbuty 1-3 7,3 8,3 9,40,41,42-hexahydroxycalix[6]arene (XXIV); 2,8,14,20,26,32-Hexa(4-chloro)phenyl-5,11,17,23,29, 35 - hexa-tertbutyl-37,38,39,40,41,42-hexahydroxycalix[6]arene ( XXV); 2,8,14,20,26,32-hexa(3,4-dimethoxy)phenyl-5,l 1,17,23,29, 35 hexatertbutyl- 37,38,39,40,41,42-hexahydroxycalix[6]arene (XXVI); 2,8,14,20-tetra (4-dimethylamino) phenyl - 5,11,17,23 tetra- tertbutyl 25,26,27,28-tetrahydroxycalix [4] arene (XXVII); 2,8,14,20- tetra (2,4,6- trimethoxy) phenyl -5,11,17,23 tetra-tertbutyl 25,26,27,28- tetrahydroxycalix [4] arene (XXVIII); 2,8,14,20- tetra (3,4,5,- trimethoxy) phenyl - 5,11,17,23 tetra-tertbutyl 25,26,27,28- tetrahydroxycalix [4] arene (XXIX), in presence of K2CO3 under microwave irradiation.

机译：本发明涉及一种制备2,8,14,20,26,32,38,44,50,56，-十（2-硝基）苯基-5,11,17,23,29,35的新方法，41,47,53,59-叔叔丁基-61,62,63,64,65,66,67,68,69,70-十羟基杯[10]芳烃（XVI）; 2,8,14,20,26,32,38,44,50,56，-十（3-硝基）苯基-5,11,17,23,29,35,41,47,53,59-十-叔丁基-61,62,63,64,65,66，67，68，69,70-十羟基杯[10]芳烃（XVII）; 2,8,14,20,26,32,38,44,50,56-十（4-硝基）苯基-5，l 1,17,23,29,35,41,47，53,59-十-叔丁基-61,62,63,64,65,66,67，68，69,70-十羟基杯[10]芳烃（XVIII）; 2,8,14,20,26,32,38,44,50,56-十（4-氰基）苯基-5,11,17,23,29,35,41,47,53,59-十-叔丁基-61,62,63,64,65,66,67，68，69,70-十羟基杯[10]芳烃（XIX）; 2,8,14,20,26,32,38,44-八（4-氟）苯基-5,11ž17,23,29,35,41,47-辛酸叔丁基49,50,51,52,53,54， 55,56-八羟基杯[8]芳烃（XX）; 2,8,14,20,26,32,38,44-八（4-甲氧基）苯基-5,11,17,23,29,35,41,47-八叔丁基49,50,51， 52，54,55,56，八羟基杯[8]芳烃（XXI）; 2,8,14,20,26,32,38,44-八（3-甲氧基）苯基-5,11ž17,23,29,35,41,47-八叔丁基49,50,51,52,53 ，54,55,56-八羟基杯[8]芳烃（XXII）; 2,8,14,20,26,32,38,44-八苯基-5,11,17,23,29,35,41,47-八叔丁基49,50,51,52,53,54 ，55,56-八羟基杯[8]芳烃（XXIII）; 2,8,14,20,26,32-六（3-氯）苯基-5,1 1,17,23,29，35-六叔丁基1-3 7,3 8,3 9,40,41 ，42-六羟基杯[6]芳烃（XXIV）; 2,8,14,20,26,32-六（4-氯）苯基-5,11,17,23,29,35-六叔丁基-37,38,39,40,41,42-六羟基杯[ 6]芳烃（XXV）; 2,8,14,20,26,32-六（3,4-二甲氧基）苯基-5,1 1,17,23,29，35六叔丁基-37,38,39,40,41,42-六羟基杯[ 6]芳烃（XXVI）; 2,8,14,20-四（4-二甲基氨基）苯基-5,11,17,23四叔丁基25,26,27,28-四羟基杯[4]芳烃（XXVII）; 2,8,14,20-四（2,4,6-三甲氧基）苯基-5,11,17,23四叔丁基25,26,27,28-四羟基杯[4]芳烃（XXVIII）; 2,8,14,20-四（3,4,5，-三甲氧基）苯基-5,11,17,23四叔丁基25,26,27,28-四羟基杯[4]芳烃（XXIX），在存在下微波辐射下的碳酸钾

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公开/公告号IN201621001392A

专利类型
公开/公告日2017-10-27

原文格式PDF
申请/专利权人
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申请/专利号IN201621001392
发明设计人 DR RATHOD S V;DR M M V RAMANA;DR RAJE M S;
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申请日2016-01-14
分类号G03G5/00;
国家 IN
入库时间 2022-08-21 13:38:35

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