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GRAPHENE DOMAIN MEASUREMENT SYSTEM AND METHOD USING AFM FRICTION MAPPING

机译:使用原子力显微镜摩擦映射的石墨烯测量系统和方法

摘要

The present invention relates to a graphene domain measurement system and method using AFM friction mapping, in which a graphene sample is rotated clockwise and is measured in order to allow the rotation angle from an initial measurement point to the final measurement point to be more than 180°; the same graphene sample is measured several times, e.g. at least five times, while the graphene sample is rotated clockwise; it is analyzed that the shading difference of the obtained friction mapping image relates to the direction in which the AFM tip progresses and the wrinkle direction of the graphene; and thus, the wrinkle direction of the graphene is obtained. In order to achieve the above goal, the present invention includes: measuring a graphene sample through an AFM microscope set to a Friction Mode, by using a measurement unit; adjusting a contrast range to the periphery of the graphene sample while an output unit outputs a friction mapping image; using the output unit to output a friction profile graph with respect to a specific portion obtained by horizontally cutting the friction mapping image; analyzing a relation between the direction in which the AFM tip progresses and the wrinkle direction of the graphene by using the friction profile graph; and determining the wrinkle direction of the graphene by using a contrast shading difference between each domain through the friction mapping image while using information analyzed by the determination unit.
机译:本发明涉及一种使用AFM摩擦映射的石墨烯域测量系统和方法,其中石墨烯样品被顺时针旋转并被测量以便允许从初始测量点到最终测量点的旋转角大于180° °;多次测量同一石墨烯样品,例如至少五次,同时将石墨烯样品顺时针旋转;分析所获得的摩擦映射图像的阴影差异与AFM尖端前进的方向和石墨烯的褶皱方向有关。因此,获得了石墨烯的皱纹方向。为了实现上述目的,本发明包括:通过使用测量单元,通过设置为摩擦模式的AFM显微镜来测量石墨烯样品;在输出单元输出摩擦映射图像的同时,调节与石墨烯样品的周围的对比度范围;使用输出单元输出相对于通过水平切割摩擦映射图像而获得的特定部分的摩擦轮廓图;通过使用摩擦曲线图分析AFM尖端的前进方向与石墨烯的皱纹方向之间的关系;通过利用摩擦映射图像利用每个区域之间的对比度阴影差来确定石墨烯的皱纹方向,同时使用确定单元所分析的信息。

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