首页> 外国专利> A METHOD FOR SYNTHESIS OF INGOING BILLETS OF CORUNDUM IN THE FORM OF POLYCRYSTALLINE INGOTS FOR GROWING CRYSTALS OF SAPPHIRE AND INSTALLATION THEREFORE

A METHOD FOR SYNTHESIS OF INGOING BILLETS OF CORUNDUM IN THE FORM OF POLYCRYSTALLINE INGOTS FOR GROWING CRYSTALS OF SAPPHIRE AND INSTALLATION THEREFORE

机译:一种合成蓝宝石长晶的多晶锭形式刚玉的入坯方法及其安装方法

摘要

The invention relates to a method for synthesis of ingoing billets of corundum in the form of polycrystalline ingots for growing crystals of sapphire, comprising introduction of a fusion mixture of aluminum oxide powder into a cold crucible, creating a high-frequency electromagnetic field with an inductor and initial melting of the fusion mixture, heating the melt in the high-frequency electromagnetic field of the inductor, feeding an additional portion of the fusion mixture in the cold crucible and its melting, crystallization the melt in the form of a polycrystalline ingot during a vertical shifting of the cold crucible with respect to the inductor, termination of the induction melting by switching off the high-frequency field of the inductor, cooling the polycrystalline ingot in the cold crucible, removing the polycrystalline ingot from the cold crucible and repeating the whole cycle from the introduction of the fusion mixture into the cold crucible and its initial melting, characterized in that after termination of the induction melting and switching off the high-frequency field of the inductor, the cold crucible (5) with the polycrystalline ingot (16) is taken out of the inductor (4) and in its place a second identical cold crucible (6) is introduced and the cycle is repeated to obtain another polycrystalline ingot (17) in the second identical cold crucible (6), wherein the cooling of the previously produced polycrystalline ingot (16) is carried out simultaneously with the synthesis of the next polycrystalline ingot (17) and removing the polycrystalline ingot (16) from the cold crucible (5) is carried out after the induction melting of the next polycrystalline ingot (17) has been terminated. The invention covers also an installation for carrying out this method.
机译:本发明涉及一种用于合成蓝宝石晶体的多晶锭形式的刚玉坯的合成方法,该方法包括将氧化铝粉末的熔融混合物引入冷坩埚中,并利用感应器产生高频电磁场。熔化混合物的初始熔化,在感应器的高频电磁场中加热熔化物,将另外一部分熔化混合物送入冷坩埚中并熔化,在熔化过程中使熔化物以多晶锭的形式结晶冷坩埚相对于感应器的垂直移动,通过关闭感应器的高频场终止感应熔化,冷却冷坩埚​​中的多晶锭,从冷坩埚中取出多晶锭,然后重复整个过程从将熔融混合物引入冷坩埚及其最初熔化的特性开始其原因在于,在感应熔化终止并关闭感应器的高频场之后,将具有多晶锭(16)的冷坩埚(5)从感应器(4)中取出,并在第二个相同的位置引入冷坩埚(6),并重复该循环,以在第二相同的冷坩埚(6)中获得另一个多晶锭(17),其中,先前制备的多晶锭(16)的冷却与硅的合成同时进行。在下一个多晶锭(17)的感应熔化终止之后,进行下一个多晶锭(17)并从冷坩埚(5)中移出多晶锭(16)。本发明还包括用于执行该方法的设备。

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