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SYSTEM OF THE LOW-TEMPERATURE CONDENSATION OF THE STEAM-GAS MIXTURE

机译:蒸汽-气体混合物的低温冷凝系统

摘要

The invention relates to a polycrystalline silicon production area, in particular to equipment for condensing the low-temperature gas mixture, formed on the portion of trichlorosilane synthesis. Developed cryogenic condensation system of the steam-gas mixture formed in the area of ​​synthesis of trichlorosilane, connected in a gas phase with the primary condensing system vapor mixture, comprising two cooled recuperative heat exchanger, the inputs of which via conduits capable of connecting to the gas phase to the system main condensation, cooling is applied CCGT mixture, condenser, cooled by liquid nitrogen to which said recuperative those communicated through conduits by gas phase ploobmenniki at least one container for collecting condensate, which by means of conduits communicate recuperative heat exchangers and the condenser, at least one tank for storing liquid nitrogen, in communication via a conduit with a capacitor, wherein the pipes are fitted with a controlled shut-off valves and recuperative heat exchanger are connected by the gas phase to the main system condensing the gas-vapor mixture in parallel to each other, wherein for cooling the gas-vapor mixture in a recuperative heat bmennike used vaporized stream of nitrogen while cooling the condenser, and the second indirect heat exchanger - the return flow of cooled gas. Thus, the inventive system is a low-temperature condensation of vapor-gas mixture through the optimal selection of the Elements, and also ensure the most efficient communication between these elements enables efficient condensation of chlorosilanes from gas-vapor mixture, efficient recovery of cold gaseous refrigerant in the recuperative heat exchangers, simplification of the construction in general and reduced cost of the system cryogenic condensation.
机译:本发明涉及一种多晶硅生产领域,特别是涉及一种在三氯硅烷合成部分上形成的用于冷凝低温气体混合物的设备。在三氯硅烷的合成区域中形成的蒸汽-气体混合物的低温冷凝系统的开发,在气相中与一级冷凝系统的蒸气混合物相连,包括两个冷却的换热器,其输入通过能够连接的导管到气相至系统的主要冷凝液,采用CCGT混合液,冷凝器进行冷却,并由液氮冷却,所述回收液通过气相ploobmenniki通过导管与至少一个用于收集冷凝液的容器进行热交换,这些容器通过导管进行热量回收交换器和冷凝器,至少一个用于储存液氮的罐,通过导管与电容器连通,其中,管道装有可控截止阀,而换热器通过气相与主系统冷凝连接气体-蒸汽混合物彼此平行,其中,为了冷却气体-气体混合物bmennike在冷却冷凝器和第二个间接热交换器-冷却后的气体回流时使用了蒸发的氮气流。因此,本发明的系统是通过元素的最佳选择进行的蒸气-气体混合物的低温冷凝,并且还确保了这些元素之间的最有效的连通使得能够从气体-蒸气混合物中有效地冷凝氯硅烷,有效地回收了冷气态。换热热交换器中的制冷剂,总体上简化了结构,降低了系统低温冷凝的成本。

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