首页> 外国专利> METHOD FOR PRODUCING ZIRCONIUM PHOSPHATE POWDER COATED WITH ANTIMICROBIAL INGREDIENT AND POWDER CONTAINING ANTIMICROBIAL INGREDIENT

METHOD FOR PRODUCING ZIRCONIUM PHOSPHATE POWDER COATED WITH ANTIMICROBIAL INGREDIENT AND POWDER CONTAINING ANTIMICROBIAL INGREDIENT

机译:一种制备有抗菌成分的粉末状磷酸锆粉及含有抗菌成分的粉末的方法

摘要

The present invention relates to a method for producing zirconium phosphate powder coated with an antimicrobial ingredient, including the steps of: (A) putting zirconium phosphate (Zr(HPO4)2.nH2O) which has been pulverized to a size of 500nm or less through a basket mill and dispersed in deionized water into a reactor, and stirring the content of the reactor at a temperature of 20 to 60°C for 0.2 to 1 hours so as to disperse the content; (B) forming antimicrobial zirconium phosphate by reacting the content with a solution obtained by dissolving silver ion precursor and a metal salt selected from the group of zinc, calcium and copper in deionized water for 12 to 48 hours; (C) filtering the zirconium phosphate of step (B), cleansing the filtered matter with deionized water, and drying the cleansed matter at a temperature of 45 to 120°C for 4 to 12 hours with hot air supplied by a far-infrared ray dryer; and (D) pulverizing and pyrolyzing the dried matter at a temperature of 250 to 300°C for 0.5 to 1 hours, and then at a temperature of 450 to 500℃ for 1 to 2 hours so as to coat the zirconium phosphate with the antimicrobial ingredient.
机译:本发明涉及一种涂覆有抗菌成分的磷酸锆粉末的制造方法,包括以下步骤:(A)放入磷酸锆(Zr(HPO 4 2 (nH 2 O)已通过篮式粉碎机粉碎至500nm或更小并分散在去离子水中到反应器中,并在20至60的温度下搅拌反应器中的物料°C 0.2至1小时以分散内容物; (B)通过使所述内容物与通过将银离子前体和选自锌,钙和铜的金属盐的溶液溶解在去离子水中12至48小时而形成抗菌磷酸锆。 (C)过滤步骤(B)的磷酸锆,用去离子水清洗滤过的物质,并用由远红外线提供的热空气在45-120℃的温度下将清洗过的物质干燥4-12小时。烘干机(D)将干燥物在250至300℃的温度下粉碎并热解0.5至1小时,然后在450至500℃的温度下粉碎1至2小时,以用抗菌剂涂覆磷酸锆。成分。

著录项

  • 公开/公告号WO2014046336A1

    专利类型

  • 公开/公告日2014-03-27

    原文格式PDF

  • 申请/专利权人 ACT CO. LTD;

    申请/专利号WO2012KR08830

  • 发明设计人 LEE WON KU;CHEON JONG WOO;YOO DAE SUNG;

    申请日2012-10-26

  • 分类号C01G5/00;B01J2/00;

  • 国家 WO

  • 入库时间 2022-08-21 15:50:46

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