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METHOD FOR PRODUCING ZIRCONIUM PHOSPHATE POWDER COATED WITH ANTIMICROBIAL INGREDIENT AND POWDER CONTAINING ANTIMICROBIAL INGREDIENT
METHOD FOR PRODUCING ZIRCONIUM PHOSPHATE POWDER COATED WITH ANTIMICROBIAL INGREDIENT AND POWDER CONTAINING ANTIMICROBIAL INGREDIENT
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机译:一种制备有抗菌成分的粉末状磷酸锆粉及含有抗菌成分的粉末的方法
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摘要
The present invention relates to a method for producing zirconium phosphate powder coated with an antimicrobial ingredient, including the steps of: (A) putting zirconium phosphate (Zr(HPO4)2.nH2O) which has been pulverized to a size of 500nm or less through a basket mill and dispersed in deionized water into a reactor, and stirring the content of the reactor at a temperature of 20 to 60°C for 0.2 to 1 hours so as to disperse the content; (B) forming antimicrobial zirconium phosphate by reacting the content with a solution obtained by dissolving silver ion precursor and a metal salt selected from the group of zinc, calcium and copper in deionized water for 12 to 48 hours; (C) filtering the zirconium phosphate of step (B), cleansing the filtered matter with deionized water, and drying the cleansed matter at a temperature of 45 to 120°C for 4 to 12 hours with hot air supplied by a far-infrared ray dryer; and (D) pulverizing and pyrolyzing the dried matter at a temperature of 250 to 300°C for 0.5 to 1 hours, and then at a temperature of 450 to 500℃ for 1 to 2 hours so as to coat the zirconium phosphate with the antimicrobial ingredient.
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