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METHOD FOR PRODUCING COMPOSITE LITHIUM IRON PHOSPHATE MATERIAL AND COMPOSITE LITHIUM IRON PHOSPHATE MATERIAL PRODUCED THEREBY
METHOD FOR PRODUCING COMPOSITE LITHIUM IRON PHOSPHATE MATERIAL AND COMPOSITE LITHIUM IRON PHOSPHATE MATERIAL PRODUCED THEREBY
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机译:磷酸铁锂复合材料的制备方法及其所生产的磷酸铁锂复合材料
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摘要
A method for producing a composite lithium iron phosphate material, which comprises formulating lithium iron phosphate material and purified water at a weight ratio of 1:5-15 into a suspension solution, slowly adjusting the pH value of the suspension solution to 1-3 with phosphoric acid at a concentration of 5-30%, adding an analytically pure soluble chloride in an amount of 0.05 - 2% based on the molar amount of the lithium iron phosphate material; then adding ammonia water into the solution to adjust the pH value of the solution to 5-6 to obtain hydroxide colloid; drying liquid through spraying to prepare powder, and calcining at 300-450°C for 3-6 hours under an inert atmosphere; coating the oxide with high conductivity obtained by thermally decomposing the hydroxide colloid on the surface of the lithium iron phosphate material grains; ball milling and sieving the calcined material into a finished product. Also disclosed is the composite lithium iron phosphate material produced by such a method.
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