首页> 外国专利> TITANIUM OXIDE SOL AND PROCESS FOR PRODUCING SAME, ULTRAFINE PARTICULATE TITANIUM OXIDE, PROCESS FOR PRODUCING SAME, AND USES OF SAME

TITANIUM OXIDE SOL AND PROCESS FOR PRODUCING SAME, ULTRAFINE PARTICULATE TITANIUM OXIDE, PROCESS FOR PRODUCING SAME, AND USES OF SAME

机译:氧化钛溶胶及其制备方法,超细微粒二氧化钛,制备方法及用途

摘要

The present invention relates to a method for producing titanium oxide sol, comprising mixing an aqueous titanium tetrachloride solution into water at a temperature of 80°C or higher within 60 seconds while maintaining the mixed solution at the temperature and cooling it to less than 60°C within 15 minutes after the mixing is completed in a method for producing titanium oxide sol by the hydrolysis of titanium tetrachloride in the liquid phase method; the highly-dispersive ultrafine particulate titanium oxide sol obtained by the method, wherein an average primal particle diameter (D BET ) calculated from the BET specific surface area is 3 to 8 nm, the cumulative 50% volume particle diameter (D50 DLS ) measured by the dynamic light scattering method and D BET have the relationship represented by D50 DLS = k x D BET (k in the formula is a value of 1 or more and less than 5) and the anatase content is 70% or more; the ultrafine particulate titanium oxide obtained by drying the titanium oxide sol; and the production method and use thereof. The ultrafine particulate titanium oxide according to the present invention is suitable for use in the photocatalyst, solar cell, dielectric material, material for the electrode of lithium ion batteries, and the like without requiring specific pulverizing treatment or dispersing agent and has a great value industrially.
机译:生产二氧化钛溶胶的方法技术领域本发明涉及一种生产二氧化钛溶胶的方法,该方法包括在60秒内将四氯化钛水溶液在80℃或更高的温度下混合到水中,同时将混合溶液保持在该温度并将其冷却至小于60°。通过液相法四氯化钛的水解来制造氧化钛溶胶的方法,在混合结束后的15分钟以内进行C。通过该方法获得的高度分散的超细颗粒状二氧化钛溶胶,其中由BET比表面积计算的平均初始粒径(D BET)为3至8nm,累积的50%体积粒径(D50 DLS)通过动态光散射法与D BET的关系为D50 DLS = k×D BET(式中的k为1以上且小于5),锐钛矿含量为70%以上。干燥钛氧化物溶胶得到的超细颗粒状氧化钛。及其生产方法和用途。根据本发明的超细颗粒状二氧化钛不需要特殊的粉碎处理或分散剂就适用于光催化剂,太阳能电池,介电材料,锂离子电池的电极材料等,并且在工业上具有很大的价值。 。

著录项

  • 公开/公告号EP2527299A4

    专利类型

  • 公开/公告日2013-11-20

    原文格式PDF

  • 申请/专利权人 SHOWA DENKO K.K.;

    申请/专利号EP20110814382

  • 发明设计人 MIZUE KEI;KAYAMA SUSUMU;

    申请日2011-06-24

  • 分类号C01G23/053;C01G23/047;H01L31/04;H01M4/485;H01M14;

  • 国家 EP

  • 入库时间 2022-08-21 15:49:11

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