首页> 外国专利> METHOD FOR PRODUCING SYNTHETIC HYDROXYAPATITE NANOPLATES AND NANOPOWDER CONTAINING SYNTHETIC HYDROXYAPATITE NANOPLATE

METHOD FOR PRODUCING SYNTHETIC HYDROXYAPATITE NANOPLATES AND NANOPOWDER CONTAINING SYNTHETIC HYDROXYAPATITE NANOPLATE

机译:合成羟基磷灰石纳米粉的制备方法和含有纳米羟基磷灰石的纳米粉

摘要

The method according to the invention relates to hydroxyapatite with a hexagonal structure. It includes a step of the precursor preparation in a form of homogeneous mixture of the suspension of calcium hydroxide in water and phosphoric acid, and a step of forming of crystalline nanostructures in such precursor. During the step of crystalline nanostructures formation the prepared precursor is subjected to microwave radiation having a power density in the range from 1 to 10 watts per 1 cm3 of the precursor for a period of 10 to 900 seconds. The nanopowder featured in the invention has the average size of nanonoplates, determined by the longest chord of the outline as a result of the designation of the particle size distribution during the dark-field imagining in the transmission electron microscope and its fitting to the resulting Gaussian distribution graph, in the range of 3 to 30 nm.
机译:根据本发明的方法涉及具有六边形结构的羟基磷灰石。它包括以氢氧化钙在水和磷酸中的悬浮液的均匀混合物形式制备前体的步骤,以及在这种前体中形成晶体纳米结构的步骤。在形成晶体纳米结构的步骤期间,使所制备的前体经受微波辐射,该微波辐射的功率密度为每1 cm3前体1至10瓦特,范围为10至900秒。本发明特征的纳米粉具有纳米板的平均尺寸,其由轮廓的最长弦决定,这是由于在透射电子显微镜中进行暗场成像期间对其进行粒径分布的指定以及其与所得高斯拟合的结果。分布图,范围为3到30 nm。

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