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HIGH CRYSTALLINE TIOF2 AND METHOD OF PREPARING THEREOF

机译:高晶态TIOF2及其制备方法

摘要

Disclosed are a high crystalline TIOF2 and a method of preparing the same. According to the present invention, the method of preparing a high crystalline TIOF2 includes: a first step (1) of preparing a titanium dioxide precursor solution by mixing an alcohol and a titanium dioxide precursor; a second step (2) of adjusting a pH by adding an acid to a solution obtained through the first step; a third step (3) of gelling a mixture solution obtained through the second step; and a fourth step (4) of preparing TIOF2 by settling a resultant mixture obtained through the third step in a reactor and injecting a nitrogen trifluoride to the reactor to react with the resultant mixture. The present invention can provide a high crystalline TIOF2 with a uniform shape in a nano-size by even a simple process.;COPYRIGHT KIPO 2014
机译:公开了一种高结晶的TIOF2及其制备方法。根据本发明,制备高结晶度TIOF 2的方法包括:第一步(1),通过将醇和二氧化钛前体混合来制备二氧化钛前体溶液。第二步(2),通过向第一步得到的溶液中加入酸来调节pH。第三步骤(3),将通过第二步骤获得的混合溶液胶凝;第四步骤(4),通过将通过第三步骤获得的所得混合物沉降到反应器中,并将三氟化氮注入反应器中以与所得混合物反应来制备TIOF2。本发明甚至可以通过简单的方法提供具有纳米尺寸的均匀形状的高结晶TIOF2。; COPYRIGHT KIPO 2014

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