首页> 外国专利> Method for evaporative crystallization of maltitol

Method for evaporative crystallization of maltitol

机译:麦芽糖醇蒸发结晶的方法

摘要

Process for preparing maltitol crystals by evaporative crystallization, characterized in that it consists of a) preparing a solution of maltitol of at least 85% richness in maltitol in dry base, preferably between 89% and 99% richness in maltitol in dry base , even more preferably comprised between 93% and 95% of dry maltitol richness, b) concentrate in partial vacuum between 20 and 30 kPa said maltitol solution, of richness between 93 and 95%, at a cooking temperature comprised between 75 and 85%, in the evaporative crystallizer so as to obtain a maltitol syrup whose degree of supersaturation in maltitol is located in the metastable zone of maltitol, c) sow the solution supersaturated in maltitol with seed crystals of maltitol in the form dispersed, d) carry out the crystallization for a total time of less than 2 hours, keeping constant the degree of supersaturation in maltitol in the area metastable thereof by controlling the temperature between 70 and 85 ° C, strong agitation by pumping the evaporation vapors, by successive steps constituted by a concentration phase by external evaporation, then a resting phase called condensation (evaporation internal), at a constant global concentration, and feed the maltitol syrup to crystallize, e) recover the crystals thus obtained.
机译:通过蒸发结晶制备麦芽糖醇晶体的方法,其特征在于它包括:a)制备麦芽糖醇在干基中的至少85%的浓度,优选在干基麦芽糖醇中的至少89%至99%的浓度,甚至更多的麦芽糖醇溶液。麦芽糖醇溶液优选在干麦芽糖醇含量的93%至95%之间,b)在蒸煮温度在75%至85%之间的蒸煮温度下,在所述部分麦芽糖醇溶液中浓缩,所述麦芽糖醇溶液的浓缩度在93%至95%之间。结晶器以获得麦芽糖醇糖浆,其麦芽糖醇中的过饱和度位于麦芽糖醇的亚稳态区,c)播种在麦芽糖醇中过饱和的溶液,其中麦芽糖醇的晶种呈分散形式,d)进行总结晶。少于2小时的时间,通过将温度控制在70至85°C之间,保持其在亚稳态麦芽糖醇中的过饱和度恒定,通过搅打进行强烈搅拌通过连续的浓缩步骤(通过外部蒸发浓缩阶段),然后以恒定的整体浓度对称为浓缩阶段(内部蒸发)的静止阶段进行平馏,然后向麦芽糖醇糖浆进料结晶,e)回收由此获得的晶体。

著录项

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号