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SAMPLE HOLDER FOR MALDI MASS SPECTROMETRIC ANALYSIS, AND MASS SPECTROMETRIC ANALYSIS METHOD

机译:MALDI质谱分析的样品夹和质谱分析方法

摘要

Used is a sample holder for MALDI mass spectrometry, which has a CuO secondary particle as a laser-beam-absorbing matrix and in which the secondary particle comprises an aggregate of CuO primary particles having an average particle diameter of 100 nm or smaller and has an uneven surface arising from the shape formed by the primary particles constituting the outermost surface of the secondary particle. As the CuO secondary particle, usable is one derived from a CuO powder produced by baking basic copper carbonate in air at 200 to 300°C, and the basic copper carbonate is produced in a process of mixing an aqueous ammonium hydrogencarbonate solution and an aqueous copper nitrate solution. The CuO secondary particle has an average particle diameter of, for example, from 0.3 to 10 µm.
机译:使用的是用于MALDI质谱的样品架,该样品架具有CuO次级粒子作为激光束吸收基质,并且其中该次级粒子包含平均粒径为100 nm或更小的CuO初级粒子的聚集体。由构成次级颗粒的最外表面的初级颗粒形成的形状引起的不平坦表面。作为CuO二次粒子,可以使用从在空气中200〜300℃下烧成碱性碳酸铜而得到的CuO粉末中得到的一种,该碱性碳酸铜是在碳酸氢铵水溶液和铜水溶液混合的过程中生成的。硝酸盐溶液。 CuO二次粒子的平均粒径例如为0.3〜10μm。

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